Ru(CO)Cl(CHCHC₆H₅)((CH₃)2C₃HNNH)(P(C₆H₄CH₃)3)2

Base Information

Chemical Name:Ru(CO)Cl(CHCHC₆H₅)((CH₃)2C₃HNNH)(P(C₆H₄CH₃)3)2
CAS No.:108296-48-6
Molecular Formula:C₅₆H₅₇ClN₂OP₂Ru
Molecular Weight:972.552
Hs Code.:

Ru(CO)Cl(CHCHC<sub>6</sub>H<sub>5</sub>)((CH<sub>3</sub>)2C<sub>3</sub>HNNH)(P(C<sub>6</sub>H<sub>4</sub>CH<sub>3</sub>)3)2

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Suppliers and Price of Ru(CO)Cl(CHCHC₆H₅)((CH₃)2C₃HNNH)(P(C₆H₄CH₃)3)2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ru(CO)Cl(CHCHC₆H₅)((CH₃)2C₃HNNH)(P(C₆H₄CH₃)3)2

Chemical Property:

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Technology Process of Ru(CO)Cl(CHCHC₆H₅)((CH₃)2C₃HNNH)(P(C₆H₄CH₃)3)2

There total 2 articles about Ru(CO)Cl(CHCHC₆H₅)((CH₃)2C₃HNNH)(P(C₆H₄CH₃)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 106564-60-7
{Ru(CO)ClH(3,5-dimethylpyrazole)(P(p-tolyl)3)2}

: 536-74-3
phenylacetylene

: 108296-48-6
Ru(CO)Cl(CHCHC₆H₅)((CH₃)2C₃HNNH)(P(C₆H₄CH₃)3)2

Guidance literature:: In dichloromethane; an excess of phenylacetylene was added to a soln. of the Ru complex, the mixt. was refluxed for 2 h, then concd., CH2Cl2 and petroleum ether were added, the ppt. was sepd., washed with EtOH and petroleum ether; purified by recrystallization from CH2Cl2 and petroleum ether; identified by elem. anal., IR and NMR spectra;

Reference yield:

: 106564-60-7
{Ru(CO)ClH(3,5-dimethylpyrazole)(P(p-tolyl)3)2}

: 536-74-3
phenylacetylene

: 108296-48-6
((p-tolyl)3P)2(3,5-dimethylpyrazole)(CO)ClRuCHCHPh

Guidance literature:: In dichloromethane; reflux, 4 h; pptn. with pentane, filtn., washing with EtOH and pentane, recrystn. from CH2Cl2/n-pentane; elem. anal.;
DOI:10.1021/om00099a014