1L-O⁴-(2,3-bis-ethoxycarbonylamino-O⁴-methyl-α-D-2,3-dideoxy-xylopyranosyl)-N,N'-bis-ethoxycarbonyl-O⁶-(6-ethoxycarbonylamino-2,3-ethoxycarbonylazanediyl-α-D-ribo-2,3,4,6-tetradeoxy-hexopyranosyl)-2-deoxy-streptamine

Base Information

• Chemical Name: 1L-O⁴-(2,3-bis-ethoxycarbonylamino-O⁴-methyl-α-D-2,3-dideoxy-xylopyranosyl)-N,N'-bis-ethoxycarbonyl-O⁶-(6-ethoxycarbonylamino-2,3-ethoxycarbonylazanediyl-α-D-ribo-2,3,4,6-tetradeoxy-hexopyranosyl)-2-deoxy-streptamine
• CAS No.: 68594-12-7
• Molecular Formula: C₃₆H₆₀N₆O₁₈
• Molecular Weight: 864.902

Synonyms:

Chemical Property of 1L-O⁴-(2,3-bis-ethoxycarbonylamino-O⁴-methyl-α-D-2,3-dideoxy-xylopyranosyl)-N,N'-bis-ethoxycarbonyl-O⁶-(6-ethoxycarbonylamino-2,3-ethoxycarbonylazanediyl-α-D-ribo-2,3,4,6-tetradeoxy-hexopyranosyl)-2-deoxy-streptamine

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 1L-O⁴-(2,3-bis-ethoxycarbonylamino-O⁴-methyl-α-D-2,3-dideoxy-xylopyranosyl)-N,N'-bis-ethoxycarbonyl-O⁶-(6-ethoxycarbonylamino-2,3-ethoxycarbonylazanediyl-α-D-ribo-2,3,4,6-tetradeoxy-hexopyranosyl)-2-deoxy-streptamine

There total 2 articles about 1L-O⁴-(2,3-bis-ethoxycarbonylamino-O⁴-methyl-α-D-2,3-dideoxy-xylopyranosyl)-N,N'-bis-ethoxycarbonyl-O⁶-(6-ethoxycarbonylamino-2,3-ethoxycarbonylazanediyl-α-D-ribo-2,3,4,6-tetradeoxy-hexopyranosyl)-2-deoxy-streptamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1L-O4-(2,3-bis-ethoxycarbonylamino-O4-methyl-α-D-2,3-dideoxy-xylopyranosyl)-O6-[2,6-bis-ethoxycarbonylamino-O3-(toluene-4-sulfonyl)-α-D-xylo-2,4,6-trideoxy-hexopyranosyl]-N,N'-bis-ethoxycarbonyl-2-deoxy-streptamine (64960-98-1) → 1L-O4-(2,3-bis-ethoxycarbonylamino-O4-methyl-α-D-2,3-dideoxy-xylopyranosyl)-N,N'-bis-ethoxycarbonyl-O6-(6-ethoxycarbonylamino-2,3-ethoxycarbonylazanediyl-α-D-ribo-2,3,4,6-tetradeoxy-hexopyranosyl)-2-deoxy-streptamine (68594-12-7)

Guidance literature:

With sodium tetrahydroborate; In dimethyl sulfoxide;

DOI:10.1246/bcsj.51.3553

Reference yield:

chloroformic acid ethyl ester (541-41-3) + 1D-O4-(2,3-azanediyl-6-ethoxycarbonylamino-α-D-ribo-2,3,4,6-tetradeoxy-hexopyranosyl)-O6-(2,3-bis-ethoxycarbonylamino-O4-methyl-α-D-2,3-dideoxy-xylopyranosyl)-N,N'-bis-ethoxycarbonyl-2-deoxy-streptamine (68594-13-8) → 1L-O4-(2,3-bis-ethoxycarbonylamino-O4-methyl-α-D-2,3-dideoxy-xylopyranosyl)-N,N'-bis-ethoxycarbonyl-O6-(6-ethoxycarbonylamino-2,3-ethoxycarbonylazanediyl-α-D-ribo-2,3,4,6-tetradeoxy-hexopyranosyl)-2-deoxy-streptamine (68594-12-7)

Guidance literature:

With sodium carbonate; In N,N-dimethyl-formamide;

DOI:10.1246/bcsj.51.3553

upstream raw materials:

chloroformic acid ethyl ester

1D-O⁴-(2,3-azanediyl-6-ethoxycarbonylamino-α-D-ribo-2,3,4,6-tetradeoxy-hexopyranosyl)-O⁶-(2,3-bis-ethoxycarbonylamino-O⁴-methyl-α-D-2,3-dideoxy-xylopyranosyl)-N,N'-bis-ethoxycarbonyl-2-deoxy-streptamine

1L-O⁴-(2,3-bis-ethoxycarbonylamino-O⁴-methyl-α-D-2,3-dideoxy-xylopyranosyl)-O⁶-[2,6-bis-ethoxycarbonylamino-O³-(toluene-4-sulfonyl)-α-D-xylo-2,4,6-trideoxy-hexopyranosyl]-N,N'-bis-ethoxycarbonyl-2-deoxy-streptamine

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