α-pipitzol benzoate

Base Information

Chemical Name:α-pipitzol benzoate
CAS No.:10067-43-3
Molecular Formula:C₂₂H₂₄O₄
Molecular Weight:352.43
Hs Code.:

Synonyms:

Suppliers and Price of α-pipitzol benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of α-pipitzol benzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of α-pipitzol benzoate

There total 1 articles about α-pipitzol benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-88-4
benzoyl chloride

: 10067-43-3,10067-44-4
β-pipitzol benzoate

Guidance literature:: With alkali;

Reference yield:

: 10067-43-3,10067-44-4
α-pipitzol benzoate

: 469-61-4
alpha-cedrene

Guidance literature:: Multi-step reaction with 7 steps

1: 13.8 g / Et₂O*BF₃ / 96 h / Ambient temperature

2: W-7 Raney Ni / ethanol / 5 h / Heating

3: Et₂O*BF₃ / 5 h / Ambient temperature

4: Raney Ni / ethanol / 5 h / Heating

5: 400 mg / aq. NaHCO₃ / methanol / 3 h / Heating

6: 150 mg / NaBH₄ / methanol / 3 h / Ambient temperature

7: 60 mg / POCl₃ / pyridine; ethanol / 19 h / 0 °C / Heating

With sodium tetrahydroborate; boron trifluoride diethyl etherate; sodium hydrogencarbonate; trichlorophosphate; W-7 Raney Ni; nickel; In pyridine; methanol; ethanol;
DOI:10.1016/S0040-4020(01)93686-5

Reference yield:

: 10067-43-3,10067-44-4
α-pipitzol benzoate

: 13794-73-5
(3R,3aR,6S,7S,8aS)-3,6,8,8-tetramethylhexahydro-1H-3a,7-cedaran-5(4H)-one

Guidance literature:: Multi-step reaction with 5 steps

1: 13.8 g / Et₂O*BF₃ / 96 h / Ambient temperature

2: W-7 Raney Ni / ethanol / 5 h / Heating

3: Et₂O*BF₃ / 5 h / Ambient temperature

4: Raney Ni / ethanol / 5 h / Heating

5: 400 mg / aq. NaHCO₃ / methanol / 3 h / Heating

With boron trifluoride diethyl etherate; sodium hydrogencarbonate; W-7 Raney Ni; nickel; In methanol; ethanol;
DOI:10.1016/S0040-4020(01)93686-5