[4-(acetyl-{4-[4-(3-acetylamino-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy]-2,3,5,6-tetrahydroxy-hexyl}-amino)-phenyl]-carbamic acid benzyl ester

Base Information

• Chemical Name: [4-(acetyl-{4-[4-(3-acetylamino-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy]-2,3,5,6-tetrahydroxy-hexyl}-amino)-phenyl]-carbamic acid benzyl ester
• CAS No.: 1053609-77-0
• Molecular Formula: C₃₆H₅₁N₃O₁₈
• Molecular Weight: 813.81

Synonyms:

Chemical Property of [4-(acetyl-{4-[4-(3-acetylamino-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy]-2,3,5,6-tetrahydroxy-hexyl}-amino)-phenyl]-carbamic acid benzyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [4-(acetyl-{4-[4-(3-acetylamino-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy]-2,3,5,6-tetrahydroxy-hexyl}-amino)-phenyl]-carbamic acid benzyl ester

There total 2 articles about [4-(acetyl-{4-[4-(3-acetylamino-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy]-2,3,5,6-tetrahydroxy-hexyl}-amino)-phenyl]-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4-Amino-phenyl)-carbamic acid benzyl ester (82720-42-1) → [4-(acetyl-{4-[4-(3-acetylamino-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy]-2,3,5,6-tetrahydroxy-hexyl}-amino)-phenyl]-carbamic acid benzyl ester (1053609-77-0)

Guidance literature:

Multi-step reaction with 3 steps

1: NaCNBH₃ / ethanol; H₂O; acetic acid / 48 h

2: ethanol; H₂O; acetic acid / 5 h

3: re. N. meningitidis β-(1-3)-N-acetylglucosaminyltransferase; bovine serum albumin (BSA) / 120 h / 20 °C / pH 7.3

With re. N. meningitidis β-(1-3)-N-acetylglucosaminyltransferase; sodium cyanoborohydride; bovine serum albumin; In ethanol; water; acetic acid; 1: reductive amination / 2: Acetylation / 3: glycosylation;

DOI:10.1016/S0008-6215(00)00128-2

Reference yield:

{4-[(2S,3R,4R,5R)-2,3,5,6-Tetrahydroxy-4-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexylamino]-phenyl}-carbamic acid benzyl ester (1053653-28-3) → [4-(acetyl-{4-[4-(3-acetylamino-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy]-2,3,5,6-tetrahydroxy-hexyl}-amino)-phenyl]-carbamic acid benzyl ester (1053609-77-0)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol; H₂O; acetic acid / 5 h

2: re. N. meningitidis β-(1-3)-N-acetylglucosaminyltransferase; bovine serum albumin (BSA) / 120 h / 20 °C / pH 7.3

With re. N. meningitidis β-(1-3)-N-acetylglucosaminyltransferase; bovine serum albumin; In ethanol; water; acetic acid; 1: Acetylation / 2: glycosylation;

DOI:10.1016/S0008-6215(00)00128-2

Reference yield:

[4-(acetyl-{4-[4-(3-acetylamino-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy]-2,3,5,6-tetrahydroxy-hexyl}-amino)-phenyl]-carbamic acid benzyl ester (1053609-77-0) → C50H74N4O28 (314075-37-1)

Guidance literature:

Multi-step reaction with 2 steps

1: recombinant bovine milk β-(1->4)-galactosyltransferase / 48 h / 20 °C / pH 7.3

2: re. N. meningitidis β-(1-3)-N-acetylglucosaminyltransferase; bovine serum albumin (BSA) / 120 h / 20 °C / pH 7.3

With re. N. meningitidis β-(1-3)-N-acetylglucosaminyltransferase; recombinant bovine milk β-(1->4)-galactosyltransferase; bovine serum albumin; 1: glycosylation / 2: glycosylation;

DOI:10.1016/S0008-6215(00)00128-2

upstream raw materials:

(4-Amino-phenyl)-carbamic acid benzyl ester

{4-[(2S,3R,4R,5R)-2,3,5,6-Tetrahydroxy-4-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexylamino]-phenyl}-carbamic acid benzyl ester

Downstream raw materials:

C₅₀H₇₄N₄O₂₈

C₅₆H₈₄N₄O₃₃

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