C₂₉H₂₆Si

Base Information

Chemical Name:C₂₉H₂₆Si
CAS No.:1373402-67-5
Molecular Formula:C₂₉H₂₆Si
Molecular Weight:402.611
Hs Code.:

Synonyms:

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Chemical Property of C₂₉H₂₆Si

Chemical Property:

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Technology Process of C₂₉H₂₆Si

There total 5 articles about C₂₉H₂₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1373402-65-3
C₂₁H₂₀Si

: 1373402-67-5
C₂₉H₂₆Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-dimethyl acetamide / dichloromethane / 3 h / 0 - 45 °C / Inert atmosphere

1.2: 0.25 h / 0 - 20 °C / Inert atmosphere

2.1: di-tert-butoxydiazene / benzene / 3 h / 60 °C / Inert atmosphere

With N,N-dimethyl acetamide; di-tert-butoxydiazene; In dichloromethane; benzene;
DOI:10.1002/chem.201102318

Reference yield:

: 7073-70-3
1-bromo-2-isopropenylbenzene

: 1373402-67-5
C₂₉H₂₆Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: tert.-butyl lithium / tetrahydrofuran; pentane / 1 h / -78 °C / Inert atmosphere

1.2: 5 h / -78 - 20 °C / Inert atmosphere

2.1: N,N-dimethyl acetamide / dichloromethane / 3 h / 0 - 45 °C / Inert atmosphere

2.2: 0.25 h / 0 - 20 °C / Inert atmosphere

3.1: di-tert-butoxydiazene / benzene / 3 h / 60 °C / Inert atmosphere

With N,N-dimethyl acetamide; di-tert-butoxydiazene; tert.-butyl lithium; In tetrahydrofuran; dichloromethane; pentane; benzene;
DOI:10.1002/chem.201102318

Reference yield:

: 2142-69-0
2-bromophenyl methyl ketone

: 1373402-67-5
C₂₉H₂₆Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

2.1: tert.-butyl lithium / tetrahydrofuran; pentane / 1 h / -78 °C / Inert atmosphere

2.2: 5 h / -78 - 20 °C / Inert atmosphere

3.1: N,N-dimethyl acetamide / dichloromethane / 3 h / 0 - 45 °C / Inert atmosphere

3.2: 0.25 h / 0 - 20 °C / Inert atmosphere

4.1: di-tert-butoxydiazene / benzene / 3 h / 60 °C / Inert atmosphere

With N,N-dimethyl acetamide; di-tert-butoxydiazene; potassium tert-butylate; tert.-butyl lithium; In tetrahydrofuran; dichloromethane; pentane; benzene;
DOI:10.1002/chem.201102318