4-Methyl-N-(oct-1-yn-3-yl)benzene-1-sulfonamide

Base Information

Chemical Name:4-Methyl-N-(oct-1-yn-3-yl)benzene-1-sulfonamide
CAS No.:139372-08-0
Molecular Formula:C15H21NO2S
Molecular Weight:279.403
Hs Code.:
DSSTox Substance ID:DTXSID50569697
Nikkaji Number:J3.071.898D

Synonyms:139372-08-0;4-Methyl-N-(oct-1-yn-3-yl)benzene-1-sulfonamide;DTXSID50569697

Suppliers and Price of 4-Methyl-N-(oct-1-yn-3-yl)benzene-1-sulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of 4-Methyl-N-(oct-1-yn-3-yl)benzene-1-sulfonamide

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:279.12930009
Heavy Atom Count:19
Complexity:394

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCC(C#C)NS(=O)(=O)C1=CC=C(C=C1)C

Technology Process of 4-Methyl-N-(oct-1-yn-3-yl)benzene-1-sulfonamide

There total 3 articles about 4-Methyl-N-(oct-1-yn-3-yl)benzene-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₂₉NO₄S

: 139372-08-0
(+/-)-4-methyl-N-(oct-1-yn-3-yl)benzenesulfonamide

Guidance literature:: With hydrogenchloride; water; In ethyl acetate; at 50 ℃; for 4h;
DOI:10.1055/s-0030-1260098

Reference yield:

: 818-72-4,37911-28-7
1-Octyn-3-ol

: 139372-08-0
(+/-)-4-methyl-N-(oct-1-yn-3-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C / Cooling

2: hydrogenchloride; water / ethyl acetate / 4 h / 50 °C

With hydrogenchloride; di-isopropyl azodicarboxylate; water; triphenylphosphine; In tetrahydrofuran; ethyl acetate; 1: Mitsunobu reaction;
DOI:10.1055/s-0030-1260098

Reference yield:

: 18303-04-3
N-[(tert-butoxy)carbonyl]-4-methylbenzenesulfonamide

: 139372-08-0
(+/-)-4-methyl-N-(oct-1-yn-3-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C / Cooling

2: hydrogenchloride; water / ethyl acetate / 4 h / 50 °C

With hydrogenchloride; di-isopropyl azodicarboxylate; water; triphenylphosphine; In tetrahydrofuran; ethyl acetate; 1: Mitsunobu reaction;
DOI:10.1055/s-0030-1260098