Technology Process of C66H62Br8O20
There total 5 articles about C66H62Br8O20 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) KOt-Bu / 1.) THF, RT, 30 min, 2.) THF, reflux, 48 h
2: 95 percent / aq. NaOH / ethanol / 22 h / 65 °C
3: 100 percent / SOCl2, DMF / 5 h / Heating
4: 1.) KOt-Bu / 1.) THF, RT, 30 min, 2.) THF, RT, overnight
With
sodium hydroxide; thionyl chloride; potassium tert-butylate; N,N-dimethyl-formamide;
In
ethanol;
DOI:10.1139/v98-236
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) KOt-Bu / 1.) THF, RT, 30 min, 2.) THF, reflux, 48 h
2: 95 percent / aq. NaOH / ethanol / 22 h / 65 °C
3: 100 percent / SOCl2, DMF / 5 h / Heating
4: 1.) KOt-Bu / 1.) THF, RT, 30 min, 2.) THF, RT, overnight
With
sodium hydroxide; thionyl chloride; potassium tert-butylate; N,N-dimethyl-formamide;
In
ethanol;
DOI:10.1139/v98-236
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 95 percent / aq. NaOH / ethanol / 22 h / 65 °C
2: 100 percent / SOCl2, DMF / 5 h / Heating
3: 1.) KOt-Bu / 1.) THF, RT, 30 min, 2.) THF, RT, overnight
With
sodium hydroxide; thionyl chloride; potassium tert-butylate; N,N-dimethyl-formamide;
In
ethanol;
DOI:10.1139/v98-236
