fac-(CO)3(1,3-bis(diphenylphosphino)propane)MnOTs

Base Information

Chemical Name:fac-(CO)3(1,3-bis(diphenylphosphino)propane)MnOTs
CAS No.:148447-54-5
Molecular Formula:C₃₇H₃₃MnO₆P₂S
Molecular Weight:722.617
Hs Code.:

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Chemical Property of fac-(CO)3(1,3-bis(diphenylphosphino)propane)MnOTs

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Technology Process of fac-(CO)3(1,3-bis(diphenylphosphino)propane)MnOTs

There total 2 articles about fac-(CO)3(1,3-bis(diphenylphosphino)propane)MnOTs which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 148447-53-4
fac-tricarbonyl(1,3-bis(diphenylphosphino)propane)hydridomanganese(I)

: 104-15-4
toluene-4-sulfonic acid

: 148447-54-5
fac-(CO)3(1,3-bis(diphenylphosphino)propane)MnOTs

Guidance literature:: In dichloromethane; byproducts: hydrogen; under Ar, slight excess of acid; extn. (water), CH2Cl2 concd., addn. of hexane, cooled, filtered, washed with hexane, dried under vac.; elem. anal.;
DOI:10.1021/om00029a032

Reference yield:

: 10170-69-1
dimanganese decacarbonyl

: 104-15-4
toluene-4-sulfonic acid

: 148447-54-5
fac-(CO)3(1,3-bis(diphenylphosphino)propane)MnOTs

Guidance literature:: In not given; (Ar); using Schlenk techniques; (Organometallics 1993, 12, 1714-1719);
DOI:10.1021/om049352v

Reference yield: 85.0%

: 148447-54-5
fac-(CO)3(1,3-bis(diphenylphosphino)propane)MnOTs

: 124-41-4
sodium methylate

: fac-(CO)3(1,3-bis(diphenylphosphino)propane)MnOCH₃*0.5CH₃OH

Guidance literature:: In methanol; under Ar, stirred at room temp. for 6 h; evapn. to dryness, extn. (benzene), diluted with hexane, cooled, filtered, washed with hexane, dried under vac.; elem. anal.;
DOI:10.1021/om00029a032