(Z)-2,3-bis(N,N'-benzoylamino)maleic acid mono methyl ester

Base Information

Chemical Name:(Z)-2,3-bis(N,N'-benzoylamino)maleic acid mono methyl ester
CAS No.:360069-49-4
Molecular Formula:C₁₉H₁₆N₂O₆
Molecular Weight:368.346
Hs Code.:

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Chemical Property of (Z)-2,3-bis(N,N'-benzoylamino)maleic acid mono methyl ester

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Technology Process of (Z)-2,3-bis(N,N'-benzoylamino)maleic acid mono methyl ester

There total 1 articles about (Z)-2,3-bis(N,N'-benzoylamino)maleic acid mono methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 290346-20-2
(Z)-2,3-bis(N,N'-benzoylamino)maleic acid dimethyl ester

: 360069-49-4
(Z)-2,3-bis(N,N'-benzoylamino)maleic acid mono methyl ester

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; at 0 ℃;
DOI:10.1002/1099-0682(200107)2001:7<1675::AID-EJIC1675>3.0.CO;2-7

Reference yield: 34.0%

: 83377-35-9,80215-76-5,12354-85-7
[Rh(Cp*)(Cl)₂]₂

: 360069-49-4
(Z)-2,3-bis(N,N'-benzoylamino)maleic acid mono methyl ester

: ((C₅(CH₃)5)RhCl)2C₆H₅CONHC₂COONHCOOCH₃

Guidance literature:: With NaOMe; In methanol; CH3OH soln. of organic ligand stirred with a soln. of NaOMe in CH3OH, (Cp*RhCl2)2 added, mixt. stirred overnight; solvent removed in vacuo, redissolved in CH2Cl2, filtered under reduced pressure, recrystallized, elem. anal., only one diastereoisomer crystallized, racemate of RR and SS;
DOI:10.1002/1099-0682(200107)2001:7<1675::AID-EJIC1675>3.0.CO;2-7