bis(perfluorovinyl)phenylphosphine

Base Information

Chemical Name:bis(perfluorovinyl)phenylphosphine
CAS No.:69249-07-6
Molecular Formula:C₁₀H₅F₆P
Molecular Weight:270.114
Hs Code.:

Synonyms:

Suppliers and Price of bis(perfluorovinyl)phenylphosphine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(perfluorovinyl)phenylphosphine

Chemical Property:

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Technology Process of bis(perfluorovinyl)phenylphosphine

There total 2 articles about bis(perfluorovinyl)phenylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 811-97-2
1,1,1,2-tetrafluoroethane

: 644-97-3
Dichlorophenylphosphine

: 69249-07-6
bis(perfluorovinyl)phenylphosphine

Guidance literature:: With n-butyllithium; Yield given; Multistep reaction; 1.) Et₂O/hexane, -78 deg C, 2 h, 2.) Et₂O/hexane, -78 deg C, 2 h;
DOI:10.1039/a806535g

Reference yield:

: 598-73-2,55157-25-0
1-bromo-1,2,2-trifluoroethene

: 644-97-3
Dichlorophenylphosphine

: 69249-07-6
bis(perfluorovinyl)phenylphosphine

Guidance literature:: Multistep reaction; (i) MeLi, Et₂O, (ii) /BRN= 508189/;

Reference yield: 78.0%

: di(rhodium)tetracarbonyl dichloride

: 69249-07-6
bis(perfluorovinyl)phenylphosphine

: 521981-44-2
trans-[RhCl(CO)((PPh)(CF=CF₂)2)2]

Guidance literature:: In dichloromethane; under inert atm. to soln. (RhCl(CO)2)2 in CH2Cl2 soln. ligand in CH2Cl2 was added dropwise, mixt. was stirred at room temp. for 1 h; mixt. was evapd., residue was washed with hexane, filtered, dried in vac.; elem. anal.;
DOI:10.1039/b711825b