4-<4-Chlor-phenyl>sulfonylamino-but-1-en

Base Information

Chemical Name:4-<4-Chlor-phenyl>sulfonylamino-but-1-en
CAS No.:28394-36-7
Molecular Formula:C₁₀H₁₂ClNO₂S
Molecular Weight:245.73
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-<4-Chlor-phenyl>sulfonylamino-but-1-en

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Technology Process of 4-<4-Chlor-phenyl>sulfonylamino-but-1-en

There total 1 articles about 4-<4-Chlor-phenyl>sulfonylamino-but-1-en which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28394-36-7
4-<4-Chlor-phenyl>sulfonylamino-but-1-en

Guidance literature:: Aus 4-<4-Chlor-benzolsulfonyl>-3.6-dihydro-1-oxo-1.2-thiazin mit 2n wss.NaOH oder mit 60percentig.wss.H2SO4 oder mit sd.H2O;

Reference yield: 33.0%

: 28394-36-7
4-<4-Chlor-phenyl>sulfonylamino-but-1-en

: 6419-73-4
N-n-butyl-4-chlorobenzenesulfonamide

: (Z)-8-chloro-3,4-dihydro-2H-benzo[g][1,2]thiazocine 1,1-dioxide

Guidance literature:: With [Cp^{1-cyclohexyl-2,3,4,5-tetramethylcyclopentadienyl}RhCl₂]₂; potassium pivalate; In 1,2-dichloro-ethane; at 80 ℃; for 24h; chemoselective reaction;
DOI:10.1021/acs.orglett.0c01823

Reference yield:

: 28394-36-7
4-<4-Chlor-phenyl>sulfonylamino-but-1-en

: 100-52-7
benzaldehyde

: trans-4-chloro-1-((4-chlorophenyl)sulfonyl)-2-phenylpiperidine

: cis-4-chloro-1-((4-chlorophenyl)sulfonyl)-2-phenylpiperidine

Guidance literature:: With chloro[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]copper(I); zirconium(IV) chloride; In dichloromethane; at 40 ℃; for 24h; Overall yield = 76 percent; Overall yield = 140.6 mg; diastereoselective reaction; Sealed tube;
DOI:10.1002/aoc.5927