(+/-)-1-benzyl-3,3-cyclohexylidenediaziridine

Base Information

Chemical Name:(+/-)-1-benzyl-3,3-cyclohexylidenediaziridine
CAS No.:58010-00-7
Molecular Formula:C₁₃H₁₈N₂
Molecular Weight:202.299
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-1-benzyl-3,3-cyclohexylidenediaziridine

Chemical Property:

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Technology Process of (+/-)-1-benzyl-3,3-cyclohexylidenediaziridine

There total 7 articles about (+/-)-1-benzyl-3,3-cyclohexylidenediaziridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 100-46-9
benzylamine

: 58010-00-7,78525-62-9,78549-74-3,78549-75-4
(+/-)-1-benzyl-3,3-cyclohexylidenediaziridine

Guidance literature:: With hydroxylamine-O-sulfonic acid; In water; at 0 - 10 ℃; Inert atmosphere;
DOI:10.1021/ol202452b

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 58010-00-7,78525-62-9,78549-74-3,78549-75-4
(-)-1-benzyl-3,3-cyclohexylidenediaziridine

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine-O-sulphonic acid

With hydroxylamine-O-sulfonic acid;
DOI:10.1016/S0040-4020(01)97652-5

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 58010-00-7,78525-62-9,78549-74-3,78549-75-4
(+)-1-benzyl-3,3-cyclohexylidenediaziridine

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine-O-sulphonic acid

With hydroxylamine-O-sulfonic acid;
DOI:10.1016/S0040-4020(01)97652-5