1-[3-Methyl-5-((E)-styryl)-isoxazol-4-yl]-6-[(E)-2-(2-nitro-phenyl)-vinyl]-1,6-dihydro-pyridine-2,3,4,5-tetracarboxylic acid tetramethyl ester

Base Information

• Chemical Name: 1-[3-Methyl-5-((E)-styryl)-isoxazol-4-yl]-6-[(E)-2-(2-nitro-phenyl)-vinyl]-1,6-dihydro-pyridine-2,3,4,5-tetracarboxylic acid tetramethyl ester
• CAS No.: 130953-23-0
• Molecular Formula: C₃₃H₂₉N₃O₁₁
• Molecular Weight: 643.607

Synonyms:

Chemical Property of 1-[3-Methyl-5-((E)-styryl)-isoxazol-4-yl]-6-[(E)-2-(2-nitro-phenyl)-vinyl]-1,6-dihydro-pyridine-2,3,4,5-tetracarboxylic acid tetramethyl ester

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Technology Process of 1-[3-Methyl-5-((E)-styryl)-isoxazol-4-yl]-6-[(E)-2-(2-nitro-phenyl)-vinyl]-1,6-dihydro-pyridine-2,3,4,5-tetracarboxylic acid tetramethyl ester

There total 3 articles about 1-[3-Methyl-5-((E)-styryl)-isoxazol-4-yl]-6-[(E)-2-(2-nitro-phenyl)-vinyl]-1,6-dihydro-pyridine-2,3,4,5-tetracarboxylic acid tetramethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

[3-Methyl-5-((E)-styryl)-isoxazol-4-yl]-[(E)-3-(2-nitro-phenyl)-prop-2-en-(E)-ylidene]-amine (130786-87-7) + dimethyl acetylenedicarboxylate (762-42-5) → 1-[3-Methyl-5-((E)-styryl)-isoxazol-4-yl]-6-[(E)-2-(2-nitro-phenyl)-vinyl]-1,6-dihydro-pyridine-2,3,4,5-tetracarboxylic acid tetramethyl ester (130953-23-0)

Guidance literature:

In toluene; Heating;

DOI:10.1246/bcsj.63.1851

Reference yield:

2-nitrocinnamaldehyde (1466-88-2,66894-06-2) → 1-[3-Methyl-5-((E)-styryl)-isoxazol-4-yl]-6-[(E)-2-(2-nitro-phenyl)-vinyl]-1,6-dihydro-pyridine-2,3,4,5-tetracarboxylic acid tetramethyl ester (130953-23-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / ethanol / Heating

2: 50 percent / toluene / Heating

In ethanol; toluene;

DOI:10.1246/bcsj.63.1851

Reference yield:

4-amino-3-methyl-5-styryl isoxazole (53558-01-3) → 1-[3-Methyl-5-((E)-styryl)-isoxazol-4-yl]-6-[(E)-2-(2-nitro-phenyl)-vinyl]-1,6-dihydro-pyridine-2,3,4,5-tetracarboxylic acid tetramethyl ester (130953-23-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / ethanol / Heating

2: 50 percent / toluene / Heating

In ethanol; toluene;

DOI:10.1246/bcsj.63.1851

upstream raw materials:

[3-Methyl-5-((E)-styryl)-isoxazol-4-yl]-[(E)-3-(2-nitro-phenyl)-prop-2-en-(E)-ylidene]-amine

dimethyl acetylenedicarboxylate

4-amino-3-methyl-5-styryl isoxazole

2-nitrocinnamaldehyde

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