Technology Process of C24H24O5
There total 4 articles about C24H24O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium hydroxide / ethanol; water / 24 h / Reflux
2.1: dmap / 0.5 h / 20 °C / Cooling with ice
2.2: 24 h / 20 °C
With
dmap; potassium hydroxide;
In
ethanol; water;
DOI:10.1016/j.tet.2013.03.087
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sulfuric acid / 24 h / Reflux
2.1: potassium carbonate; potassium iodide / 24 h / Reflux; Inert atmosphere
3.1: potassium hydroxide / ethanol; water / 24 h / Reflux
4.1: dmap / 0.5 h / 20 °C / Cooling with ice
4.2: 24 h / 20 °C
With
dmap; sulfuric acid; potassium carbonate; potassium iodide; potassium hydroxide;
In
ethanol; water;
DOI:10.1016/j.tet.2013.03.087
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate; potassium iodide / 24 h / Reflux; Inert atmosphere
2.1: potassium hydroxide / ethanol; water / 24 h / Reflux
3.1: dmap / 0.5 h / 20 °C / Cooling with ice
3.2: 24 h / 20 °C
With
dmap; potassium carbonate; potassium iodide; potassium hydroxide;
In
ethanol; water;
DOI:10.1016/j.tet.2013.03.087