C₁₃H₁₄O₃

Base Information

Chemical Name:C₁₃H₁₄O₃
CAS No.:1322546-87-1
Molecular Formula:C₁₃H₁₄O₃
Molecular Weight:218.252
Hs Code.:

C<sub>13</sub>H<sub>14</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₁₃H₁₄O₃

Chemical Property:

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Technology Process of C₁₃H₁₄O₃

There total 5 articles about C₁₃H₁₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 140840-85-3
3-(((tert-butyldimethylsilyl)oxy)methyl)cyclopent-2-en-1-one

: 1322546-87-1
C₁₃H₁₄O₃

Guidance literature:: Multi-step reaction with 3 steps

1: 1,1′-binaphthalene-2,2′-diylbis[bis(4-methylphenyl)phosphine]; copper(l) chloride; sodium t-butanolate / 91 h / 0 - 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

3: triethylamine; dmap / tetrahydrofuran / 20 °C

With dmap; tetrabutyl ammonium fluoride; 1,1′-binaphthalene-2,2′-diylbis[bis(4-methylphenyl)phosphine]; triethylamine; copper(l) chloride; sodium t-butanolate; In tetrahydrofuran;
DOI:10.1016/j.tetasy.2013.02.015

Reference yield:

: 1322546-79-1
tert-butyl(dimethyl){[1-(phenylsulfonyl)cyclopent-3-en-1-yl]methoxy}silane

: 1322546-87-1
C₁₃H₁₄O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: borane-THF / tetrahydrofuran / 1.42 h / 0 °C

1.2: 1 h / 0 °C

2.1: sodium hydrogencarbonate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium bromide; sodium hypochlorite / water; dichloromethane / 1 h / 0 °C

3.1: triethylamine / tetrahydrofuran / 2 h / 50 °C

4.1: (S)-DTBM-SEGPHOS; copper(II) acetate monohydrate / toluene / 3 h / 20 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

6.1: triethylamine; dmap / tetrahydrofuran / 20 °C

With dmap; sodium hypochlorite; borane-THF; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; (S)-DTBM-SEGPHOS; tetrabutyl ammonium fluoride; copper(II) acetate monohydrate; sodium hydrogencarbonate; triethylamine; potassium bromide; In tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1016/j.tetasy.2013.02.015

Reference yield:

: 1322546-76-8
C₁₂H₁₄O₃S

: 1322546-87-1
C₁₃H₁₄O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 15 h / 20 °C

2.1: borane-THF / tetrahydrofuran / 1.42 h / 0 °C

2.2: 1 h / 0 °C

3.1: sodium hydrogencarbonate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium bromide; sodium hypochlorite / water; dichloromethane / 1 h / 0 °C

4.1: triethylamine / tetrahydrofuran / 2 h / 50 °C

5.1: (S)-DTBM-SEGPHOS; copper(II) acetate monohydrate / toluene / 3 h / 20 °C / Inert atmosphere

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

7.1: triethylamine; dmap / tetrahydrofuran / 20 °C

With 1H-imidazole; dmap; sodium hypochlorite; borane-THF; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; (S)-DTBM-SEGPHOS; tetrabutyl ammonium fluoride; copper(II) acetate monohydrate; sodium hydrogencarbonate; triethylamine; potassium bromide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tetasy.2013.02.015