rhamnocitrin-3-O-{(3S)-hydroxy-3-methyl-5-[(S)-1-phenylethylamino]glutaryl-(1->6)}-[α-L-rhamnopyranosyl-(1->2)]-β-D-galactopyranoside

Base Information

• Chemical Name: rhamnocitrin-3-O-{(3S)-hydroxy-3-methyl-5-[(S)-1-phenylethylamino]glutaryl-(1->6)}-[α-L-rhamnopyranosyl-(1->2)]-β-D-galactopyranoside
• CAS No.: 1386974-96-4
• Molecular Formula: C₄₂H₄₉NO₁₈
• Molecular Weight: 855.847
• Mol file: 1386974-96-4.mol

Synonyms:

Chemical Property of rhamnocitrin-3-O-{(3S)-hydroxy-3-methyl-5-[(S)-1-phenylethylamino]glutaryl-(1->6)}-[α-L-rhamnopyranosyl-(1->2)]-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of rhamnocitrin-3-O-{(3S)-hydroxy-3-methyl-5-[(S)-1-phenylethylamino]glutaryl-(1->6)}-[α-L-rhamnopyranosyl-(1->2)]-β-D-galactopyranoside

There total 1 articles about rhamnocitrin-3-O-{(3S)-hydroxy-3-methyl-5-[(S)-1-phenylethylamino]glutaryl-(1->6)}-[α-L-rhamnopyranosyl-(1->2)]-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-1-phenyl-ethylamine (2627-86-3) + rhamnocitrin-3-O-[(S)-3-hydroxy-3-methylglutaryl-(1->6)]-[α-L-rhamnopyranosyl-(1->2)]-β-D-galactopyranoside (1391144-80-1) → rhamnocitrin-3-O-{(3S)-hydroxy-3-methyl-5-[(S)-1-phenylethylamino]glutaryl-(1->6)}-[α-L-rhamnopyranosyl-(1->2)]-β-D-galactopyranoside (1386974-96-4)

Guidance literature:

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 9h; Cooling with ice;

DOI:10.1021/np300292f

Reference yield:

rhamnocitrin-3-O-{(3S)-hydroxy-3-methyl-5-[(S)-1-phenylethylamino]glutaryl-(1->6)}-[α-L-rhamnopyranosyl-(1->2)]-β-D-galactopyranoside (1386974-96-4) → (3R)-1-[(S)-1-phenylethyl]mevalonamide (946831-51-2)

Guidance literature:

With lithium borohydride; In tetrahydrofuran; at 20 ℃; for 24h; Cooling with ice;

DOI:10.1021/np300292f

upstream raw materials:

(S)-1-phenyl-ethylamine

rhamnocitrin-3-O-[(S)-3-hydroxy-3-methylglutaryl-(1->6)]-[α-L-rhamnopyranosyl-(1->2)]-β-D-galactopyranoside

Downstream raw materials:

(3R)-1-[(S)-1-phenylethyl]mevalonamide