(2S,3S,4S,5S)-2-((benzoyloxy)methyl)-5-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)tetrahydrofuran-3,4-diyl dibenzoate

Base Information

Chemical Name:(2S,3S,4S,5S)-2-((benzoyloxy)methyl)-5-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)tetrahydrofuran-3,4-diyl dibenzoate
CAS No.:77180-83-7
Molecular Formula:C₃₀H₂₄N₂O₉
Molecular Weight:556.529
Hs Code.:

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Chemical Property of (2S,3S,4S,5S)-2-((benzoyloxy)methyl)-5-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)tetrahydrofuran-3,4-diyl dibenzoate

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Technology Process of (2S,3S,4S,5S)-2-((benzoyloxy)methyl)-5-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)tetrahydrofuran-3,4-diyl dibenzoate

There total 15 articles about (2S,3S,4S,5S)-2-((benzoyloxy)methyl)-5-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)tetrahydrofuran-3,4-diyl dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 98-88-4
benzoyl chloride

: 58-96-8,3083-77-0,3258-07-9,3565-16-0,4348-60-1,4348-61-2,4348-71-4,4401-72-3,4433-38-9,16535-78-7,20289-55-8,20289-61-6,24259-58-3,26287-69-4,26524-61-8,36684-86-3,40093-89-8,41545-81-7,41545-82-8
1-(β-L-arabinofuranosyl)-uracil

: 1748-04-5,3258-14-8,4348-69-0,4348-70-3,20289-60-5,20397-91-5,26287-73-0,77180-84-8,77180-85-9,77180-83-7
2',3',5'-tri-O-benzoyl-ara-L-uridine

Guidance literature:: With pyridine; at 20 ℃; for 16h; Cooling with ice;
DOI:10.1080/15257770.2012.689410

Reference yield: 89.0%

: 3080-30-6,6974-32-9,14215-97-5,16162-35-9,20822-87-1,21138-42-1,22249-15-6,22249-17-8,26287-72-9,53403-35-3,53403-36-4,57236-69-8,70832-64-3,99395-04-7,100101-51-7,109668-83-9,120019-54-7
1-O-acetyl-2,3,5-tri-O-benzoyl-β-L-ribofuranose

: 66-22-8,144104-68-7,18324-22-6,27072-01-1,2920-92-5,51953-19-6
uracil

: 1748-04-5,3258-14-8,4348-69-0,4348-70-3,20289-60-5,20397-91-5,77180-83-7,77180-84-8,77180-85-9,26287-73-0
(2S,3S,4S,5S)-2-((benzoyloxy)methyl)-5-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)tetrahydrofuran-3,4-diyl dibenzoate

Guidance literature:: With benzenesulfonamide; trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 65 ℃;
DOI:10.1016/S0040-4020(98)01119-3