C₃₁H₃₆O₁₀

Base Information

Chemical Name:C₃₁H₃₆O₁₀
CAS No.:1415692-60-2
Molecular Formula:C₃₁H₃₆O₁₀
Molecular Weight:568.621
Hs Code.:

C<sub>31</sub>H<sub>36</sub>O<sub>10</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₁H₃₆O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₃₁H₃₆O₁₀

There total 6 articles about C₃₁H₃₆O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13061-96-6
dihydroxy-methyl-borane

: 1005142-67-5
(1S,3′R,4′S,5′S,6′R)-3′,4′,5′-tri(acetoxy)-6′-acetoxymethyl-5-chloro-6-[(4-ethylphenyl)methyl]-3′,4′,5′,6′-tetrahydrospiro-[isobenzofuran-1(3H),2′-[2H]pyran]

: 1415692-60-2
C₃₁H₃₆O₁₀

Guidance literature:: With potassium phosphate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tri tert-butylphosphoniumtetrafluoroborate; In 5,5-dimethyl-1,3-cyclohexadiene; at 145 ℃; for 15h;
DOI:10.1021/jm300884k

Reference yield:

: 1005142-57-3
[4-(acetoxymethyl)-2-bromo-5-chlorophenyl]methyl acetate

: 1415692-60-2
C₃₁H₃₆O₁₀

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium hydroxide; water / tetrahydrofuran; ethanol / 3 h / 80 °C

2.1: pyridinium p-toluenesulfonate / tetrahydrofuran / 2 h / 0 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.42 h / -78 °C / Inert atmosphere

3.2: 0.08 h

4.1: toluene-4-sulfonic acid / tetrahydrofuran; methanol / 15 h / 20 °C

5.1: chloro-trimethyl-silane / dimethyl sulfoxide / 4 h / 20 °C

5.2: 1 h / 0 - 20 °C

6.1: tetrabutylammomium bromide; bis(cyclopentadienyl)titanium dichloride; sodium carbonate / water; N,N-dimethyl-formamide / 15 h / 85 °C

7.1: bis(dibenzylideneacetone)-palladium⁽⁰⁾; tri tert-butylphosphoniumtetrafluoroborate; potassium phosphate / 5,5-dimethyl-1,3-cyclohexadiene / 15 h / 145 °C

With bis(cyclopentadienyl)titanium dichloride; potassium phosphate; n-butyllithium; chloro-trimethyl-silane; tetrabutylammomium bromide; water; pyridinium p-toluenesulfonate; sodium carbonate; toluene-4-sulfonic acid; potassium hydroxide; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tri tert-butylphosphoniumtetrafluoroborate; In tetrahydrofuran; methanol; 5,5-dimethyl-1,3-cyclohexadiene; ethanol; hexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm300884k

Reference yield:

: 85072-44-2
1-bromo-4-chloro-2,5-dimethylbenzene

: 1415692-60-2
C₃₁H₃₆O₁₀

Guidance literature:: Multi-step reaction with 9 steps

1.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / ethyl acetate / 0.33 h / Reflux

2.1: N,N-dimethyl-formamide / 3 h / 80 °C

3.1: potassium hydroxide; water / tetrahydrofuran; ethanol / 3 h / 80 °C

4.1: pyridinium p-toluenesulfonate / tetrahydrofuran / 2 h / 0 °C

5.1: n-butyllithium / tetrahydrofuran; hexane / 0.42 h / -78 °C / Inert atmosphere

5.2: 0.08 h

6.1: toluene-4-sulfonic acid / tetrahydrofuran; methanol / 15 h / 20 °C

7.1: chloro-trimethyl-silane / dimethyl sulfoxide / 4 h / 20 °C

7.2: 1 h / 0 - 20 °C

8.1: tetrabutylammomium bromide; bis(cyclopentadienyl)titanium dichloride; sodium carbonate / water; N,N-dimethyl-formamide / 15 h / 85 °C

9.1: bis(dibenzylideneacetone)-palladium⁽⁰⁾; tri tert-butylphosphoniumtetrafluoroborate; potassium phosphate / 5,5-dimethyl-1,3-cyclohexadiene / 15 h / 145 °C

With bis(cyclopentadienyl)titanium dichloride; potassium phosphate; N-Bromosuccinimide; n-butyllithium; chloro-trimethyl-silane; 2,2'-azobis(isobutyronitrile); tetrabutylammomium bromide; water; pyridinium p-toluenesulfonate; sodium carbonate; toluene-4-sulfonic acid; potassium hydroxide; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tri tert-butylphosphoniumtetrafluoroborate; In tetrahydrofuran; methanol; 5,5-dimethyl-1,3-cyclohexadiene; ethanol; hexane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm300884k