Technology Process of cis-2--4-hydroperoxy-6-(4-nitrophenyl)tetrahydro-2H-1,3,2-oxazaphosphorine 2-oxide
There total 2 articles about cis-2--4-hydroperoxy-6-(4-nitrophenyl)tetrahydro-2H-1,3,2-oxazaphosphorine 2-oxide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: gaseous NH3 / tetrahydrofuran; hexane / 0 °C
2: 1.) O3, 2.) 30percent aq. H2O2 / 1.) acetone, H2O, 0 deg C, 2.) acetone, H2O, RT, overnight
With
ammonia; dihydrogen peroxide; ozone;
In
tetrahydrofuran; hexane;
DOI:10.1021/jm00114a013
- Guidance literature:
-
With
dihydrogen peroxide; ozone;
Yield given. Multistep reaction;
1.) acetone, H2O, 0 deg C, 2.) acetone, H2O, RT, overnight;
DOI:10.1021/jm00114a013
