cis-2--4-hydroperoxy-6-(4-nitrophenyl)tetrahydro-2H-1,3,2-oxazaphosphorine 2-oxide

Base Information

Chemical Name:cis-2--4-hydroperoxy-6-(4-nitrophenyl)tetrahydro-2H-1,3,2-oxazaphosphorine 2-oxide
CAS No.:129253-32-3
Molecular Formula:C₁₃H₁₈Cl₂N₃O₆P
Molecular Weight:414.182
Hs Code.:

cis-2-<bis(2-chloroethyl)amino>-4-hydroperoxy-6-(4-nitrophenyl)tetrahydro-2H-1,3,2-oxazaphosphorine 2-oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-2--4-hydroperoxy-6-(4-nitrophenyl)tetrahydro-2H-1,3,2-oxazaphosphorine 2-oxide

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Technology Process of cis-2--4-hydroperoxy-6-(4-nitrophenyl)tetrahydro-2H-1,3,2-oxazaphosphorine 2-oxide

There total 2 articles about cis-2--4-hydroperoxy-6-(4-nitrophenyl)tetrahydro-2H-1,3,2-oxazaphosphorine 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₁₈Cl₃N₂O₄P

: 129253-32-3,136235-89-7
cis-2--4-hydroperoxy-6-(4-nitrophenyl)tetrahydro-2H-1,3,2-oxazaphosphorine 2-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: gaseous NH₃ / tetrahydrofuran; hexane / 0 °C

2: 1.) O₃, 2.) 30percent aq. H₂O₂ / 1.) acetone, H₂O, 0 deg C, 2.) acetone, H₂O, RT, overnight

With ammonia; dihydrogen peroxide; ozone; In tetrahydrofuran; hexane;
DOI:10.1021/jm00114a013

Reference yield:

: 136185-90-5
1-(4-nitrophenyl)-3-butenyl N,N-bis(2-chloroethyl)phosphorodiamidate

: 129253-32-3,136235-89-7
cis-2--4-hydroperoxy-6-(4-nitrophenyl)tetrahydro-2H-1,3,2-oxazaphosphorine 2-oxide

Guidance literature:: With dihydrogen peroxide; ozone; Yield given. Multistep reaction; 1.) acetone, H₂O, 0 deg C, 2.) acetone, H₂O, RT, overnight;
DOI:10.1021/jm00114a013