Epivitamin D₃-p-nitrobenzoat

Base Information

Chemical Name:Epivitamin D₃-p-nitrobenzoat
CAS No.:60413-85-6
Molecular Formula:C₃₄H₄₇NO₄
Molecular Weight:533.751
Hs Code.:

Synonyms:

Suppliers and Price of Epivitamin D₃-p-nitrobenzoat

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Epivitamin D₃-p-nitrobenzoat

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Epivitamin D₃-p-nitrobenzoat

There total 6 articles about Epivitamin D₃-p-nitrobenzoat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-97-0
vitamin D₃

: 62-23-7
4-nitro-benzoic acid

: 6183-79-5,60413-84-5,60413-85-6,62743-69-5
Epivitamin D₃-p-nitrobenzoat

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; benzene;
DOI:10.1002/hlca.19760590622

Reference yield:

: 67-97-0
vitamin D₃

: 122-04-3
4-nitro-benzoyl chloride

: 6183-79-5,60413-84-5,60413-85-6,62743-69-5
vitamin D3 p-nitrobenzoate

Guidance literature:: With pyridine;
DOI:10.1021/ja01220a033

Reference yield:

: 434-16-2
7-dehydrocholesterol

: 6183-79-5,60413-84-5,60413-85-6,62743-69-5
vitamin D3 p-nitrobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / Irradiation_.UV-Licht; unter Luftausschluss; Reinigung ueber das O-<3.5-Dinitro-benzoyl>-Derivat, das O-<3.5-Dinitro-4-methyl-benzoyl>-Derivat oder das Allophanoyl-Derivat

2: pyridine

With pyridine; diethyl ether;