Technology Process of C14H18O4
There total 2 articles about C14H18O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: magnesium chloride; triethylamine / acetonitrile / 0.25 h / 20 °C
1.2: 2 h / Reflux
2.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C
3.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C
With
di-isopropyl azodicarboxylate; potassium tert-butylate; triethylamine; triphenylphosphine; magnesium chloride;
In
tetrahydrofuran; acetonitrile;
DOI:10.1021/ja4018122
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C
2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C
With
di-isopropyl azodicarboxylate; potassium tert-butylate; triphenylphosphine;
In
tetrahydrofuran;
DOI:10.1021/ja4018122
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper dichloride; water / acetonitrile / Reflux
2: sodium tetrahydroborate / ethanol / 0 °C
With
sodium tetrahydroborate; water; copper dichloride;
In
ethanol; acetonitrile;
DOI:10.1021/ja4018122