Technology Process of C24H40F2N2O4Si
There total 10 articles about C24H40F2N2O4Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine / dichloromethane / -78 - 20 °C
2.1: 2,6-dimethylpyridine / dichloromethane
3.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water
4.1: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 75 °C
5.1: 75 °C
6.1: Wilkinson's catalyst / ethanol; water / Reflux
6.2: 20 °C / pH 10 / aq. buffer
7.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 20 °C
8.1: methanol; potassium carbonate / 20 °C
9.1: palladium on activated charcoal; hydrogen / methanol
With
2,6-dimethylpyridine; methanol; Wilkinson's catalyst; di-n-butylboryl trifluoromethanesulfonate; diphenyl phosphoryl azide; palladium on activated charcoal; hydrogen; dihydrogen peroxide; potassium carbonate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium hydroxide; diethylazodicarboxylate;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene;
4.1: Curtius rearrangement / 7.1: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2011.06.109
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 20 °C
2: methanol; potassium carbonate / 20 °C
3: palladium on activated charcoal; hydrogen / methanol
With
methanol; palladium on activated charcoal; hydrogen; potassium carbonate; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; methanol;
1: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2011.06.109
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine / dichloromethane / -78 - 20 °C
2.1: 2,6-dimethylpyridine / dichloromethane
3.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water
4.1: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 75 °C
5.1: 75 °C
6.1: Wilkinson's catalyst / ethanol; water / Reflux
6.2: 20 °C / pH 10 / aq. buffer
7.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 20 °C
8.1: methanol; potassium carbonate / 20 °C
9.1: palladium on activated charcoal; hydrogen / methanol
With
2,6-dimethylpyridine; methanol; Wilkinson's catalyst; di-n-butylboryl trifluoromethanesulfonate; diphenyl phosphoryl azide; palladium on activated charcoal; hydrogen; dihydrogen peroxide; potassium carbonate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium hydroxide; diethylazodicarboxylate;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene;
4.1: Curtius rearrangement / 7.1: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2011.06.109
