Technology Process of C16H23(2)HO3
There total 3 articles about C16H23(2)HO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 98 percent / trimethylchlorosilane, / CH2Cl2 / Heating
2: 1.) LiAlH4 2.) pyridinium dichromate / 1.) THF, 0 deg C; 2.) CH2Cl2, reflux
3: 1.) horse liver alcohol dehydrogenase, nicotinamide adenine dinucleotide, ethanol-d6 2.) NaH, / 1.) 0.05M potassium phosphate buffer (pH 8.8) 2.) N,N-dimethylformamide, room temperature
With
lithium aluminium tetrahydride; dipyridinium dichromate; chloro-trimethyl-silane; ethanol-d6; horse liver alcohol dehydrogenase; sodium hydride; nicotinamide adenine dinucleotide;
In
dichloromethane;
DOI:10.1016/S0040-4039(00)96284-1
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) LiAlH4 2.) pyridinium dichromate / 1.) THF, 0 deg C; 2.) CH2Cl2, reflux
2: 1.) horse liver alcohol dehydrogenase, nicotinamide adenine dinucleotide, ethanol-d6 2.) NaH, / 1.) 0.05M potassium phosphate buffer (pH 8.8) 2.) N,N-dimethylformamide, room temperature
With
lithium aluminium tetrahydride; dipyridinium dichromate; ethanol-d6; horse liver alcohol dehydrogenase; sodium hydride; nicotinamide adenine dinucleotide;
DOI:10.1016/S0040-4039(00)96284-1
- Guidance literature:
-
With
ethanol-d6; horse liver alcohol dehydrogenase; sodium hydride; nicotinamide adenine dinucleotide;
Yield given. Multistep reaction;
1.) 0.05M potassium phosphate buffer (pH 8.8) 2.) N,N-dimethylformamide, room temperature;
DOI:10.1016/S0040-4039(00)96284-1
