C₁₉H₃₀O₂Si

Base Information

Chemical Name:C₁₉H₃₀O₂Si
CAS No.:1314939-60-0
Molecular Formula:C₁₉H₃₀O₂Si
Molecular Weight:318.531
Hs Code.:

C<sub>19</sub>H<sub>30</sub>O<sub>2</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₉H₃₀O₂Si

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Technology Process of C₁₉H₃₀O₂Si

There total 9 articles about C₁₉H₃₀O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1314939-59-7
(+/-)-3-(t-butyldimethylsilanyloxy)-3-phenylpent-4-en-1-al

: 1826-67-1
vinyl magnesium bromide

: 1314939-60-0
C₁₉H₃₀O₂Si

Guidance literature:: In tetrahydrofuran; at -20 - 0 ℃; Inert atmosphere;
DOI:10.5012/bkcs.2011.32.5.1662

Reference yield:

: 1314939-46-2
(+/-)-5-(t-butyldimethylsilanyloxy)-3-phenylpent-1-en-3-ol

: 1314939-60-0
C₁₉H₃₀O₂Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran; acetonitrile / 0 - 20 °C / Inert atmosphere

2.1: pyridine; dmap / 0 - 20 °C / Inert atmosphere

3.1: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: ammonia / methanol / 20 °C / Inert atmosphere

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C / Inert atmosphere

5.2: 0.5 h / -78 - 0 °C / Inert atmosphere

6.1: tetrahydrofuran / -20 - 0 °C / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; dmap; oxalyl dichloride; tetrabutyl ammonium fluoride; ammonia; dimethyl sulfoxide; In tetrahydrofuran; methanol; dichloromethane; acetonitrile; 5.1: Swern oxidation / 5.2: Swern oxidation;
DOI:10.5012/bkcs.2011.32.5.1662

Reference yield:

: 1314939-49-5
(+/-)-3-phenylpent-4-ene-1,3-diol

: 1314939-60-0
C₁₉H₃₀O₂Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine; dmap / 0 - 20 °C / Inert atmosphere

2.1: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

3.1: ammonia / methanol / 20 °C / Inert atmosphere

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C / Inert atmosphere

4.2: 0.5 h / -78 - 0 °C / Inert atmosphere

5.1: tetrahydrofuran / -20 - 0 °C / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; dmap; oxalyl dichloride; ammonia; dimethyl sulfoxide; In tetrahydrofuran; methanol; dichloromethane; 4.1: Swern oxidation / 4.2: Swern oxidation;
DOI:10.5012/bkcs.2011.32.5.1662