C₄₉H₅₃FN₄O₉S₂

Base Information

Chemical Name:C₄₉H₅₃FN₄O₉S₂
CAS No.:1334138-54-3
Molecular Formula:C₄₉H₅₃FN₄O₉S₂
Molecular Weight:925.112
Hs Code.:

C<sub>49</sub>H<sub>53</sub>FN<sub>4</sub>O<sub>9</sub>S<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₉H₅₃FN₄O₉S₂

Chemical Property:

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Technology Process of C₄₉H₅₃FN₄O₉S₂

There total 11 articles about C₄₉H₅₃FN₄O₉S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1334137-74-4
tert-butyl 4-(3-hydroxy-4-methoxybenzoyl)-1-piperazinecarboxylate

: 1334138-54-3
C₄₉H₅₃FN₄O₉S₂

Guidance literature:: Multi-step reaction with 4 steps

1: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C

2: triethylamine / dichloromethane / 0 - 20 °C

3: potassium carbonate / acetone / Reflux

4: potassium carbonate / acetone / Reflux

With potassium carbonate; triethylamine; trifluoroacetic acid; In dichloromethane; acetone;
DOI:10.1002/cmdc.201100207

Reference yield:

: 1334137-72-2
(3-hydroxy-4-methoxybenzoyl)-1-piperazine

: 1334138-54-3
C₄₉H₅₃FN₄O₉S₂

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 0 - 20 °C

2: potassium carbonate / acetone / Reflux

3: potassium carbonate / acetone / Reflux

With potassium carbonate; triethylamine; In dichloromethane; acetone;
DOI:10.1002/cmdc.201100207

Reference yield:

: 1334137-76-6
C₁₉H₁₅FO₂

: 1334138-54-3
C₄₉H₅₃FN₄O₉S₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: water; sodium hydroxide / ethanol / 20 - 80 °C

1.2: pH 7

2.1: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 0 - 20 °C / Inert atmosphere

3.1: triethylamine / dichloromethane / 0 - 20 °C

4.1: potassium carbonate / acetone / Reflux

5.1: potassium carbonate / acetone / Reflux

With thionyl chloride; water; potassium carbonate; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; In ethanol; dichloromethane; acetone;
DOI:10.1002/cmdc.201100207