meso-1,4-bis(4-methoxyphenyl)-2,3-butanediol

Base Information

Chemical Name:meso-1,4-bis(4-methoxyphenyl)-2,3-butanediol
CAS No.:63035-47-2
Molecular Formula:C₁₈H₂₂O₄
Molecular Weight:302.37
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of meso-1,4-bis(4-methoxyphenyl)-2,3-butanediol

Chemical Property:

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Technology Process of meso-1,4-bis(4-methoxyphenyl)-2,3-butanediol

There total 12 articles about meso-1,4-bis(4-methoxyphenyl)-2,3-butanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.5%

: 102574-41-4
cis-2,3-bis(4-methoxybenzyl)oxirane

: 63035-47-2
meso-1,4-bis(4-methoxyphenyl)-2,3-butanediol

: 102574-43-6
d,l-1,4-bis(4-methoxyphenyl)-2,3-butanediol

Guidance literature:: With sulfuric acid; water; at 25 ℃; for 24h; Product distribution; Mechanism; other p-methoxy-substituted trans-epoxides; other reagents, other reaction times;
DOI:10.1021/jo00364a026

Reference yield:

: 63035-46-1
cis-1,4-bis(4-methoxyphenyl)-2-butene

: 63035-47-2
meso-1,4-bis(4-methoxyphenyl)-2,3-butanediol

Guidance literature:: Multistep reaction; (i) AgOAc, I₂, aq. AcOH, (ii) KOH, EtOH;
DOI:10.1021/ja00451a035

Reference yield:

: 104-01-8
4-Methoxyphenylacetic acid

: 63035-47-2
meso-1,4-bis(4-methoxyphenyl)-2,3-butanediol

Guidance literature:: Multi-step reaction with 4 steps

2: Na2(OCH₂CH₂OMe)2>

3: PhLi

4: (i) AgOAc, I₂, aq. AcOH, (ii) KOH, EtOH

With phenyllithium; sodium bis(2-methoxyethoxy)aluminium dihydride;
DOI:10.1021/ja00451a035