Acetic acid (S)-1-(7-benzyloxy-heptyl)-nonyl ester

Base Information

Chemical Name:Acetic acid (S)-1-(7-benzyloxy-heptyl)-nonyl ester
CAS No.:199382-27-9
Molecular Formula:C₂₅H₄₂O₃
Molecular Weight:390.607
Hs Code.:

Synonyms:

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Chemical Property of Acetic acid (S)-1-(7-benzyloxy-heptyl)-nonyl ester

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Technology Process of Acetic acid (S)-1-(7-benzyloxy-heptyl)-nonyl ester

There total 19 articles about Acetic acid (S)-1-(7-benzyloxy-heptyl)-nonyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 629-11-8
1,6-hexanediol

: 199382-27-9
Acetic acid (S)-1-(7-benzyloxy-heptyl)-nonyl ester

Guidance literature:: Multi-step reaction with 12 steps

1: 54 percent / NaH / tetrahydrofuran / 2 h / Heating

2: pyridine / CH₂Cl₂ / 72 h / 20 °C

3: 5.10 g / NaI; NaHCO₃ / acetone / 72 h / 20 °C

4: 83 percent / Li₂CuCl₄ / tetrahydrofuran; diethyl ether / 2 h / 0 °C

5: 88 percent / 4-methylmorpholine N-oxide; OsO₄ / H₂O; 2-methyl-propan-2-ol; acetone / 2 h / 20 °C

6: 84 percent / pyridine / CH₂Cl₂ / -78 - 0 °C

7: 24 percent

8: Et₃N; DMAP / CH₂Cl₂; toluene / 20 °C

9: pyridine; DMAP / 20 °C

10: 24.9 mg / TBAF / tetrahydrofuran / 20 °C

11: tetrahydrofuran / 3 h

12: pyridine; DMAP

With pyridine; dmap; osmium(VIII) oxide; dilithium tetrachlorocuprate; tetrabutyl ammonium fluoride; sodium hydride; sodium hydrogencarbonate; 4-methylmorpholine N-oxide; triethylamine; sodium iodide; In tetrahydrofuran; diethyl ether; dichloromethane; water; acetone; toluene; tert-butyl alcohol;
DOI:10.1016/S0040-4020(00)00904-2

Reference yield:

: 71126-73-3
6-benzyloxyhexan-1-ol

: 199382-27-9
Acetic acid (S)-1-(7-benzyloxy-heptyl)-nonyl ester

Guidance literature:: Multi-step reaction with 11 steps

1: pyridine / CH₂Cl₂ / 72 h / 20 °C

2: 5.10 g / NaI; NaHCO₃ / acetone / 72 h / 20 °C

3: 83 percent / Li₂CuCl₄ / tetrahydrofuran; diethyl ether / 2 h / 0 °C

4: 88 percent / 4-methylmorpholine N-oxide; OsO₄ / H₂O; 2-methyl-propan-2-ol; acetone / 2 h / 20 °C

5: 84 percent / pyridine / CH₂Cl₂ / -78 - 0 °C

6: 24 percent

7: Et₃N; DMAP / CH₂Cl₂; toluene / 20 °C

8: pyridine; DMAP / 20 °C

9: 24.9 mg / TBAF / tetrahydrofuran / 20 °C

10: tetrahydrofuran / 3 h

11: pyridine; DMAP

With pyridine; dmap; osmium(VIII) oxide; dilithium tetrachlorocuprate; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; 4-methylmorpholine N-oxide; triethylamine; sodium iodide; In tetrahydrofuran; diethyl ether; dichloromethane; water; acetone; toluene; tert-butyl alcohol;
DOI:10.1016/S0040-4020(00)00904-2

Reference yield:

: 97510-97-9
(((6-iodohexyl)oxy)methyl)benzene

: 199382-27-9
Acetic acid (S)-1-(7-benzyloxy-heptyl)-nonyl ester

Guidance literature:: Multi-step reaction with 9 steps

1: 83 percent / Li₂CuCl₄ / tetrahydrofuran; diethyl ether / 2 h / 0 °C

2: 88 percent / 4-methylmorpholine N-oxide; OsO₄ / H₂O; 2-methyl-propan-2-ol; acetone / 2 h / 20 °C

3: 84 percent / pyridine / CH₂Cl₂ / -78 - 0 °C

4: 24 percent

5: Et₃N; DMAP / CH₂Cl₂; toluene / 20 °C

6: pyridine; DMAP / 20 °C

7: 24.9 mg / TBAF / tetrahydrofuran / 20 °C

8: tetrahydrofuran / 3 h

9: pyridine; DMAP

With pyridine; dmap; osmium(VIII) oxide; dilithium tetrachlorocuprate; tetrabutyl ammonium fluoride; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; water; acetone; toluene; tert-butyl alcohol;
DOI:10.1016/S0040-4020(00)00904-2