[Pd(2,3-(MeO)2C6H2CH=N(Cy)-C6,N)(μ-Cl)]2

Base Information

Chemical Name:[Pd(2,3-(MeO)2C6H2CH=N(Cy)-C6,N)(μ-Cl)]2
CAS No.:494831-06-0
Molecular Formula:C₃₀H₄₀Cl₂N₂O₄Pd₂
Molecular Weight:776.405
Hs Code.:

Synonyms:

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Chemical Property of [Pd(2,3-(MeO)2C6H2CH=N(Cy)-C6,N)(μ-Cl)]2

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Technology Process of [Pd(2,3-(MeO)2C6H2CH=N(Cy)-C6,N)(μ-Cl)]2

There total 1 articles about [Pd(2,3-(MeO)2C6H2CH=N(Cy)-C6,N)(μ-Cl)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 312925-53-4
[Pd(2,3-(MeO)2C6H2CH=N(Cy)-C6,N)(μ-acetate)]2

: 7647-14-5
sodium chloride

: 494831-06-0
[Pd(2,3-(MeO)2C6H2CH=N(Cy)-C6,N)(μ-Cl)]2

Guidance literature:: In water; acetone; under Ar, 0.01 M aq. NaCl was added dropwise to Me2CO soln. of Pd-complex, stirring for 12 h; solid was filtered off, washed twice with H2O, dried in vac. over anhyd.CaCl2;
DOI:10.1039/b203864a

Reference yield: 95.0%

: ammonium hexafluorophosphate

: 494831-06-0
[Pd(2,3-(MeO)2C6H2CH=N(Cy)-C6,N)(μ-Cl)]2

: 84494-89-3
1,1-bis-(diphenylphosphino)ethene

: 494831-09-3
[Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CCH₂-P,P')]PF₆

Guidance literature:: In water; acetone; under Ar, 2 equiv. of P-compd. was added to Me2CO soln. of Pd-compd., stirring at room temp. for 30 min, NH4PF6 was added, stirring for 30 min, H2O was added, stirring for 12 h; ppt. was filtered off, washed twice with water, dried in vac. over CaCl2, recrystn. from CHCl3 by gaseous Et2O diffusion;
DOI:10.1039/b203864a

Reference yield: 95.0%

: 494831-06-0
[Pd(2,3-(MeO)2C6H2CH=N(Cy)-C6,N)(μ-Cl)]2

: sodium perchlorate

: 84494-89-3
1,1-bis-(diphenylphosphino)ethene

: 494831-11-7
[Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CCH₂-P,P')]ClO₄

Guidance literature:: In water; acetone; under Ar, 2 equiv. of P-compd. was added to Me2CO soln. of Pd-compd., stirring at room temp. for 30 min, NaClO4 was added, stirring for 30 min, H2O was added, stirring for 12 h; ppt. was filtered off, washed twice with water, dried in vac. over CaCl2, recrystn. from CHCl3 by gaseous Et2O diffusion;
DOI:10.1039/b203864a