Technology Process of 7,12-dihydro-7-tosyl-6,12-methano-2,3-methylenedioxy-6H-dibenzo<1,3>oxazocine
There total 3 articles about 7,12-dihydro-7-tosyl-6,12-methano-2,3-methylenedioxy-6H-dibenzo<1,3>oxazocine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 94 percent / p-TsOH / toluene / 2 h / Heating
2: 1.) PdCl2, LiCl / 1.) acetone, r.t., 15 min, 2.) acetone, r.t., 6 h
With
toluene-4-sulfonic acid; lithium chloride; palladium dichloride;
In
toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 98 percent / NaBH4 / methanol / 0.5 h / Ambient temperature
2: 94 percent / p-TsOH / toluene / 2 h / Heating
3: 1.) PdCl2, LiCl / 1.) acetone, r.t., 15 min, 2.) acetone, r.t., 6 h
With
sodium tetrahydroborate; toluene-4-sulfonic acid; lithium chloride; palladium dichloride;
In
methanol; toluene;
- Guidance literature:
-
With
lithium chloride; palladium dichloride;
Yield given. Multistep reaction. Yields of byproduct given;
1.) acetone, r.t., 15 min, 2.) acetone, r.t., 6 h;
