7,12-dihydro-7-tosyl-6,12-methano-2,3-methylenedioxy-6H-dibenzo<1,3>oxazocine

Base Information

Chemical Name:7,12-dihydro-7-tosyl-6,12-methano-2,3-methylenedioxy-6H-dibenzo<1,3>oxazocine
CAS No.:159682-30-1
Molecular Formula:C₂₃H₁₉NO₅S
Molecular Weight:421.474
Hs Code.:

7,12-dihydro-7-tosyl-6,12-methano-2,3-methylenedioxy-6H-dibenzo<d,g><1,3>oxazocine

Synonyms:

Suppliers and Price of 7,12-dihydro-7-tosyl-6,12-methano-2,3-methylenedioxy-6H-dibenzo<1,3>oxazocine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 7,12-dihydro-7-tosyl-6,12-methano-2,3-methylenedioxy-6H-dibenzo<1,3>oxazocine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 7,12-dihydro-7-tosyl-6,12-methano-2,3-methylenedioxy-6H-dibenzo<1,3>oxazocine

There total 3 articles about 7,12-dihydro-7-tosyl-6,12-methano-2,3-methylenedioxy-6H-dibenzo<1,3>oxazocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24206-42-6
1,2,3,4-tetrahydro-4-hydroxy-1-tosylquinoline

: 159682-30-1
7,12-dihydro-7-tosyl-6,12-methano-2,3-methylenedioxy-6H-dibenzo<1,3>oxazocine

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / p-TsOH / toluene / 2 h / Heating

2: 1.) PdCl₂, LiCl / 1.) acetone, r.t., 15 min, 2.) acetone, r.t., 6 h

With toluene-4-sulfonic acid; lithium chloride; palladium dichloride; In toluene;

Reference yield:

: 14278-37-6
1-tosyl-2,3-dihydroquinolin-4(1H)-one

: 159682-30-1
7,12-dihydro-7-tosyl-6,12-methano-2,3-methylenedioxy-6H-dibenzo<1,3>oxazocine

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / NaBH₄ / methanol / 0.5 h / Ambient temperature

2: 94 percent / p-TsOH / toluene / 2 h / Heating

3: 1.) PdCl₂, LiCl / 1.) acetone, r.t., 15 min, 2.) acetone, r.t., 6 h

With sodium tetrahydroborate; toluene-4-sulfonic acid; lithium chloride; palladium dichloride; In methanol; toluene;

Reference yield:

: 13268-54-7
1-tosyl-1, 2-dihydroquinoline

: 61080-20-4
2-(chloromercurio)-4,5-(methylenedioxy)phenol

: 159682-30-1
7,12-dihydro-7-tosyl-6,12-methano-2,3-methylenedioxy-6H-dibenzo<1,3>oxazocine

: 5,6,6a,11a-tetrahydro-5-tosyl-8,9-methylenedioxy<1>benzofuro<3,2-c>quinoline

Guidance literature:: With lithium chloride; palladium dichloride; Yield given. Multistep reaction. Yields of byproduct given; 1.) acetone, r.t., 15 min, 2.) acetone, r.t., 6 h;