Technology Process of C24H23N3O5*ClH
There total 6 articles about C24H23N3O5*ClH which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium hydroxide / 150 °C
1.2: 2 h / 170 °C
2.1: boron tribromide / dichloromethane / 0 - 20 °C
3.1: potassium hydroxide / Reflux
4.1: caesium carbonate / N,N-dimethyl-formamide / Heating
5.1: hydrogenchloride / ethyl acetate / 20 °C
With
hydrogenchloride; boron tribromide; caesium carbonate; potassium hydroxide;
In
dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.10.057
- Guidance literature:
-
Multi-step reaction with 4 steps
1: boron tribromide / dichloromethane / 0 - 20 °C
2: potassium hydroxide / Reflux
3: caesium carbonate / N,N-dimethyl-formamide / Heating
4: hydrogenchloride / ethyl acetate / 20 °C
With
hydrogenchloride; boron tribromide; caesium carbonate; potassium hydroxide;
In
dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.10.057
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium hydroxide / Reflux
2: caesium carbonate / N,N-dimethyl-formamide / Heating
3: hydrogenchloride / ethyl acetate / 20 °C
With
hydrogenchloride; caesium carbonate; potassium hydroxide;
In
ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.10.057
