N₃-Phe-Ala(4-pyridine)-Leu-NHNH₂

Base Information

Chemical Name:N₃-Phe-Ala(4-pyridine)-Leu-NHNH₂
CAS No.:1421640-03-0
Molecular Formula:C₂₃H₃₀N₈O₃
Molecular Weight:466.543
Hs Code.:

N<SUB>3</SUB>-Phe-Ala(4-pyridine)-Leu-NHNH<SUB>2</SUB>

Synonyms:

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Chemical Property of N₃-Phe-Ala(4-pyridine)-Leu-NHNH₂

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Technology Process of N₃-Phe-Ala(4-pyridine)-Leu-NHNH₂

There total 5 articles about N₃-Phe-Ala(4-pyridine)-Leu-NHNH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7517-19-3
methyl (L)-leucinate hydrochloride

: 1421640-03-0
N₃-Phe-Ala(4-pyridine)-Leu-NHNH₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2 h

2.1: trifluoroacetic acid / dichloromethane / 0.5 h

3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.08 h

3.2: 1 h

4.1: hydrazine hydrate / methanol

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm3016987

Reference yield:

: (x)C₂HF₃O₂*C₁₅H₂₃N₃O₃

: 1421640-03-0
N₃-Phe-Ala(4-pyridine)-Leu-NHNH₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.08 h

1.2: 1 h

2.1: hydrazine hydrate / methanol

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;
DOI:10.1021/jm3016987

Reference yield:

: 37535-57-2
(S)-2-((tert-butoxycarbonyl)amino)-3-(pyridin-4-yl)propanoic acid

: 1421640-03-0
N₃-Phe-Ala(4-pyridine)-Leu-NHNH₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2 h

2.1: trifluoroacetic acid / dichloromethane / 0.5 h

3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.08 h

3.2: 1 h

4.1: hydrazine hydrate / methanol

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm3016987