CrMe[N(SiMe₂CH₂PPh₂)2](SPh)

Base Information

Chemical Name:CrMe[N(SiMe₂CH₂PPh₂)2](SPh)
CAS No.:197171-53-2
Molecular Formula:C₃₇H₄₄CrNP₂SSi₂
Molecular Weight:704.944
Hs Code.:

CrMe[N(SiMe<sub>2</sub>CH<sub>2</sub>PPh<sub>2</sub>)2](SPh)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of CrMe[N(SiMe₂CH₂PPh₂)2](SPh)

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Technology Process of CrMe[N(SiMe₂CH₂PPh₂)2](SPh)

There total 1 articles about CrMe[N(SiMe₂CH₂PPh₂)2](SPh) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 158758-82-8
CrMe[N(SiMe₂CH₂PPh₂)2]

: 882-33-7
diphenyldisulfane

: 197171-53-2
CrMe[N(SiMe₂CH₂PPh₂)2](SPh)

Guidance literature:: In toluene; N2 or Ar-atmosphere; addn. of PhSSPh to soln. of Cr-complex at 0°C, stirring for 1 h, warming to room temp.; evapn., dissoln. (hexanes), filtration (Celite), evapn., recrystn. (hexanes:MePh, -40°C); elem. anal.;
DOI:10.1021/om970574l