(2Z)-[2-(4-Methylbenzene-1-sulfonyl)hydrazinylidene](phenyl)acetic acid

Base Information

Chemical Name:(2Z)-[2-(4-Methylbenzene-1-sulfonyl)hydrazinylidene](phenyl)acetic acid
CAS No.:82323-45-3
Molecular Formula:C15H14 N2 O4 S
Molecular Weight:318.353
Hs Code.:
DSSTox Substance ID:DTXSID90547717
NSC Number:239367

Synonyms:82323-45-3;SCHEMBL10782610;DTXSID90547717;NSC239367;(2Z)-[2-(4-Methylbenzene-1-sulfonyl)hydrazinylidene](phenyl)acetic acid;NSC-239367

Suppliers and Price of (2Z)-[2-(4-Methylbenzene-1-sulfonyl)hydrazinylidene](phenyl)acetic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of (2Z)-[2-(4-Methylbenzene-1-sulfonyl)hydrazinylidene](phenyl)acetic acid

Chemical Property:

Vapor Pressure:1.31E-11mmHg at 25°C
Boiling Point:519.3°C at 760 mmHg
Flash Point:267.9°C
Density:1.32g/cm³
XLogP3:3.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:5
Exact Mass:318.06742811
Heavy Atom Count:22
Complexity:510

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)NN=C(C2=CC=CC=C2)C(=O)O
Isomeric SMILES:CC1=CC=C(C=C1)S(=O)(=O)N/N=C(/C2=CC=CC=C2)\C(=O)O

Technology Process of (2Z)-[2-(4-Methylbenzene-1-sulfonyl)hydrazinylidene](phenyl)acetic acid

There total 1 articles about (2Z)-[2-(4-Methylbenzene-1-sulfonyl)hydrazinylidene](phenyl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 611-73-4
Benzoylformic acid

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 82323-45-3
2-oxophenylacetic acid tosylhydrazone

Guidance literature:: With hydrogenchloride; In methanol; for 0.0833333h; Heating;
DOI:10.1021/jo00139a002

Reference yield: 76.3%

: 82323-45-3
2-oxophenylacetic acid tosylhydrazone

: 82323-46-4
phenylglyoxylic acid chloride p-toluenesulfonylhydrazone

Guidance literature:: With thionyl chloride; In benzene; for 1.5h; Heating;
DOI:10.1021/jo00139a002

Reference yield:

: 82323-45-3
2-oxophenylacetic acid tosylhydrazone

: 82323-36-2
cis-2-(2-hydroxypropyl)-1,2-diphenylcyclopropane-1-carboxylic acid lactone

Guidance literature:: Multi-step reaction with 3 steps

1: 76.3 percent / thionyl chloride / benzene / 1.5 h / Heating

2: 93.4 percent / triethylamine / CH₂Cl₂ / 6 h / 0 deg C to 25 deg C

3: 85.1 percent / copper-bronze / benzene / 1 h / Heating

With thionyl chloride; copper; triethylamine; In dichloromethane; benzene;
DOI:10.1021/jo00139a002