2-((R)-2,2,6-Trimethyl-cyclohexyl)-ethanol

Base Information

Chemical Name:2-((R)-2,2,6-Trimethyl-cyclohexyl)-ethanol
CAS No.:124462-87-9
Molecular Formula:C₁₁H₂₂O
Molecular Weight:170.295
Hs Code.:

Synonyms:

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Chemical Property of 2-((R)-2,2,6-Trimethyl-cyclohexyl)-ethanol

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Technology Process of 2-((R)-2,2,6-Trimethyl-cyclohexyl)-ethanol

There total 4 articles about 2-((R)-2,2,6-Trimethyl-cyclohexyl)-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124177-09-9
ethyl (1R,3S)-3-hydroxy-2,2-dimethyl-6-methylenecyclohexaneacetate

: 124462-87-9
2-((R)-2,2,6-Trimethyl-cyclohexyl)-ethanol

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / LiAlH₄ / CH₂Cl₂ / 20 h / Ambient temperature

2: 98 percent / NEt₃ / CH₂Cl₂ / 20 h / Ambient temperature

3: 1. n-butyllithium, N,N,N',N'-tetramethylethylendiamine / 1. n-hexane, 1,2-dimethoxyethane, 2 h, room temperature 2. 20 h, room temperature

4: 1. Li, t-BuOH 2. 48percent aq. HF / 1. -78 deg C, THF, 1 h 2. acetonitrile, 1 h, room temperature

With lithium aluminium tetrahydride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; hydrogen fluoride; lithium; triethylamine; tert-butyl alcohol; In dichloromethane;

Reference yield:

: 124462-82-4
(1R,3S)-2-(-)-3-hydroxy-2,2-dimethyl-6-methylene-1-cyclohexaneethanol

: 124462-87-9
2-((R)-2,2,6-Trimethyl-cyclohexyl)-ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / NEt₃ / CH₂Cl₂ / 20 h / Ambient temperature

2: 1. n-butyllithium, N,N,N',N'-tetramethylethylendiamine / 1. n-hexane, 1,2-dimethoxyethane, 2 h, room temperature 2. 20 h, room temperature

3: 1. Li, t-BuOH 2. 48percent aq. HF / 1. -78 deg C, THF, 1 h 2. acetonitrile, 1 h, room temperature

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; hydrogen fluoride; lithium; triethylamine; tert-butyl alcohol; In dichloromethane;

Reference yield:

: 124462-83-5
(1S,2R)-(-)-3-<2'-(tert-butyldimethylsilyloxy)ethyl>-2,2-dimethyl-4-methylene-1-cyclohexanol

: 124462-87-9
2-((R)-2,2,6-Trimethyl-cyclohexyl)-ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1. n-butyllithium, N,N,N',N'-tetramethylethylendiamine / 1. n-hexane, 1,2-dimethoxyethane, 2 h, room temperature 2. 20 h, room temperature

2: 1. Li, t-BuOH 2. 48percent aq. HF / 1. -78 deg C, THF, 1 h 2. acetonitrile, 1 h, room temperature

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; hydrogen fluoride; lithium; tert-butyl alcohol;