C₅₃H₈₄N₆O₁₄

Base Information

• Chemical Name: C₅₃H₈₄N₆O₁₄
• CAS No.: 1379598-44-3
• Molecular Formula: C₅₃H₈₄N₆O₁₄
• Molecular Weight: 1029.28
• Mol file: 1379598-44-3.mol

Synonyms:

Chemical Property of C₅₃H₈₄N₆O₁₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₃H₈₄N₆O₁₄

There total 3 articles about C₅₃H₈₄N₆O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(2-AMINOETHYL)MORPHOLINE (2038-03-1) + 2-((2R,5S,8R,11S,14R,17S,20R,23S)-14-benzyl-5,11,17,23-tetraisobutyl-4,8,16,22-hexamethyl-3,6,9,12,15,18,21,24-octaoxo-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclo-tetracosan-2-yl)acetic acid (189131-13-3) → C53H84N6O14 (1379598-44-3)

Guidance literature:

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃;

DOI:10.1271/bbb.110129

Reference yield:

C60H82N4O14 (189159-97-5) → C53H84N6O14 (1379598-44-3)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 3.5 h / 20 °C

2: benzotriazol-1-ol; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C

With palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol;

DOI:10.1271/bbb.110129

Reference yield:

PF1022A antipode (133413-70-4) → C53H84N6O14 (1379598-44-3)

Guidance literature:

Multi-step reaction with 2 steps

1: ruthenium trichloride; periodic acid / tetrachloromethane; water / 20 °C

2: benzotriazol-1-ol; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C

With ruthenium trichloride; benzotriazol-1-ol; periodic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; tetrachloromethane; water;

DOI:10.1271/bbb.110129

upstream raw materials:

4-(2-AMINOETHYL)MORPHOLINE

2-((2R,5S,8R,11S,14R,17S,20R,23S)-14-benzyl-5,11,17,23-tetraisobutyl-4,8,16,22-hexamethyl-3,6,9,12,15,18,21,24-octaoxo-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclo-tetracosan-2-yl)acetic acid

C₆₀H₈₂N₄O₁₄

PF1022A antipode