diphenyl(κ2-tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide)platinum(II)

Base Information

Chemical Name:diphenyl(κ2-tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide)platinum(II)
CAS No.:1352287-04-7
Molecular Formula:C₃₆H₂₈N₉OPPt
Molecular Weight:828.732
Hs Code.:

Synonyms:

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Chemical Property of diphenyl(κ2-tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide)platinum(II)

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Technology Process of diphenyl(κ2-tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide)platinum(II)

There total 2 articles about diphenyl(κ2-tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide)platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 133892-27-0
tetraphenylbis(dimethyl sulfide)diplatinum(II)

: 1035346-89-4
tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide

: 1352287-04-7
diphenyl(κ2-tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide)platinum(II)

Guidance literature:: In dichloromethane; under N2; CH2Cl2 added to Pt complex and ligand; stirred at room temp. for 30 min; solvent evapd.; purified by flash chromy. (alumina, ethyl acetate, MeOH); MeOH fraction collected; solvent removed by rotary evapn.; elem. anal.;
DOI:10.1021/om2007997

Reference yield: 56.0%

: 64827-26-5
cis-{Pt2(Ph)4-bis(μ-diethyl sulphide)}

: 1035346-89-4
tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide

: 1352287-04-7
diphenyl(κ2-tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide)platinum(II)

Guidance literature:: In dichloromethane; (N2); using Schlenk techniques; placing of (Pt(SEt2)Ph2)2 and tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide in Schlenk flask under N2, addn. of CH2Cl2 through septum, stirring for 30 min at room temp.; evapn. of solvent, flash chromy. on alumina, treatment with EtOAc and then by MeOH, collection of methanol eluent, removal of solvent by rotary evapn.; elem. anal.;
DOI:10.1021/om2010595

Reference yield:

: 1352287-04-7
diphenyl(κ2-tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide)platinum(II)

: 1354482-83-9
[(κ3-tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide)PtH(CH2CH2-o-C6H4)]BF4

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane

2: chloroform-d1

In chloroform-d1; dichloromethane;
DOI:10.1021/om2010595