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(((CH3)2CH)2C6H3NC(CH3)CHC(CH3)NC6H3(CH(CH3)2)2)GeF

Base Information
  • Chemical Name:(((CH3)2CH)2C6H3NC(CH3)CHC(CH3)NC6H3(CH(CH3)2)2)GeF
  • CAS No.:382150-85-8
  • Molecular Formula:C29H41FGeN2
  • Molecular Weight:509.246
  • Hs Code.:
(((CH<sub>3</sub>)2CH)2C<sub>6</sub>H<sub>3</sub>NC(CH<sub>3</sub>)CHC(CH<sub>3</sub>)NC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2)GeF

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Chemical Property of (((CH3)2CH)2C6H3NC(CH3)CHC(CH3)NC6H3(CH(CH3)2)2)GeF
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Technology Process of (((CH3)2CH)2C6H3NC(CH3)CHC(CH3)NC6H3(CH(CH3)2)2)GeF

There total 1 articles about (((CH3)2CH)2C6H3NC(CH3)CHC(CH3)NC6H3(CH(CH3)2)2)GeF which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In dichloromethane; byproducts: Me3SnCl; under N2, standard Schlenk techniques; soln. of Ge compd. in CH2Cl2 added to stirred suspn. of Me3SnF (molar ratio 1:1.1) in CH2Cl2; stirred at room temp. for 2 d; volatiles removed; extd. with n-hexane; stored at -32°C for 24 h;elem. anal.;
DOI:10.1021/om010358j
Guidance literature:
In toluene; byproducts: N2; under N2, standard Schlenk techniques; soln. of Ge compd. and Me3SiN3 (molar ratio 1:1) in toluene refluxed for 3 h; volatiles removed; washed with n-hexane; soln. stored at -32°C; elem. anal.;
DOI:10.1021/om010358j
Guidance literature:
In toluene; soln. of Ge-compound in toluene was added to suspn. of S in toluene, stirred for 2 d under N2; filtered, stored at -32°C for 24 h;
DOI:10.1039/b211617k
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