(η5-4-Ph-7-Ph-C9H5)TiCl3

Base Information

• Chemical Name: (η5-4-Ph-7-Ph-C9H5)TiCl3
• CAS No.: 196793-69-8
• Molecular Formula: C₂₁H₁₅Cl₃Ti
• Molecular Weight: 421.589
• Mol file: 196793-69-8.mol

Synonyms:

Chemical Property of (η5-4-Ph-7-Ph-C9H5)TiCl3

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of (η5-4-Ph-7-Ph-C9H5)TiCl3

There total 1 articles about (η5-4-Ph-7-Ph-C9H5)TiCl3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

C21H15Si(CH3)3 (951152-39-9) + titanium tetrachloride (7550-45-0) → (η5-4-Ph-7-Ph-C9H5)TiCl3 (196793-69-8)

Guidance literature:

In toluene; byproducts: Me3SiCl; organic ligand dissolved in toluene and cooled to -30°C; TiCl4 intoluene added dropwise in 3 min; warmed to 25°C; stirred for 12 h; volatiles evapd.; washed 3 times with n-pentane; toluene added; filtered; solvent evapd.; elem. anal.;

DOI:10.1515/znb-2007-0811

upstream raw materials:

C₂₁H₁₅Si(CH₃)3

titanium tetrachloride

Refernces