C₅₂H₇₀N₁₀O₉

Base Information

Chemical Name:C₅₂H₇₀N₁₀O₉
CAS No.:258873-65-3
Molecular Formula:C₅₂H₇₀N₁₀O₉
Molecular Weight:979.189
Hs Code.:

C<sub>52</sub>H<sub>70</sub>N<sub>10</sub>O<sub>9</sub>

Synonyms:

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Chemical Property of C₅₂H₇₀N₁₀O₉

Chemical Property:

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Technology Process of C₅₂H₇₀N₁₀O₉

There total 10 articles about C₅₂H₇₀N₁₀O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 145013-05-4
tert-butyl N-({[(tert-butoxy)carbonyl]amino}methanethioyl)carbamate

: 258873-64-2
(3S,7S)-3,7-Diamino-5-[2-(1-trityl-1H-imidazol-2-yl)-ethyl]-[1,5]diazocan-2-one

: 258873-65-3
C₅₂H₇₀N₁₀O₉

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1055/s-1999-2969

Reference yield:

: 23593-68-2
2-methyl-1-tritylimidazole

: 258873-65-3
C₅₂H₇₀N₁₀O₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-BuLi / tetrahydrofuran / 0.83 h / -78 °C

1.2: 87 percent / tetrahydrofuran / 0.25 h / -78 °C

2.1: CHCl₃; ethanol / 3 h / 20 °C

3.1: NaBH₃CN; AcOH / CHCl₃; ethanol / 3 h

4.1: HCl / dioxane; CH₂Cl₂ / 2 h / 0 °C

5.1: Et₃N; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / tetrahydrofuran / 3 h / 20 °C

With hydrogenchloride; n-butyllithium; sodium cyanoborohydride; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; chloroform; 1.1: Metallation / 1.2: Substitution / 2.1: Condensation / 3.1: Reduction / 4.1: Substitution / 5.1: Condensation;
DOI:10.1055/s-1999-2969

Reference yield:

: (2S,6R)-2,6-Diamino-tetrahydro-pyrazolo[1,2-a]pyrazol-1-one

: 258873-65-3
C₅₂H₇₀N₁₀O₉

Guidance literature:: Multi-step reaction with 6 steps

1: Na₂CO₃ / tetrahydrofuran / 20 °C

2: 92 percent / Raney Ni / propan-2-ol / 1 h / 50 °C

3: CHCl₃; ethanol / 3 h / 20 °C

4: NaBH₃CN; AcOH / CHCl₃; ethanol / 3 h

5: HCl / dioxane; CH₂Cl₂ / 2 h / 0 °C

6: Et₃N; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / tetrahydrofuran / 3 h / 20 °C

With hydrogenchloride; nickel; sodium cyanoborohydride; sodium carbonate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; chloroform; isopropyl alcohol; 1: Acylation / 2: Reduction / 3: Condensation / 4: Reduction / 5: Substitution / 6: Condensation;
DOI:10.1055/s-1999-2969