N-p-tolyl-3a,4,5,7a-tetrahydro-5,7a-epoxy-3,4-propanoisoindoline

Base Information

Chemical Name:N-p-tolyl-3a,4,5,7a-tetrahydro-5,7a-epoxy-3,4-propanoisoindoline
CAS No.:108181-33-5
Molecular Formula:C₁₈H₂₁NO
Molecular Weight:267.371
Hs Code.:

Synonyms:

Suppliers and Price of N-p-tolyl-3a,4,5,7a-tetrahydro-5,7a-epoxy-3,4-propanoisoindoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-p-tolyl-3a,4,5,7a-tetrahydro-5,7a-epoxy-3,4-propanoisoindoline

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Technology Process of N-p-tolyl-3a,4,5,7a-tetrahydro-5,7a-epoxy-3,4-propanoisoindoline

There total 4 articles about N-p-tolyl-3a,4,5,7a-tetrahydro-5,7a-epoxy-3,4-propanoisoindoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 3139-27-3
N-((furane-2-yl)methyl)-4-methylbenzeneamine

: 1521-51-3,113667-32-6
rac-3-bromocyclohexene

: 108181-33-5
N-p-tolyl-3a,4,5,7a-tetrahydro-5,7a-epoxy-3,4-propanoisoindoline

: 108181-32-4
cyclohex-2-enyl-furan-2-ylmethyl-p-tolyl-amine

Guidance literature:: With In(OSO₂CF₃)3; for 0.133333h; Irradiation; microwave;
DOI:10.1016/S0040-4039(00)01513-6

Reference yield: 15.0%

: 108181-32-4
cyclohex-2-enyl-furan-2-ylmethyl-p-tolyl-amine

: 108181-33-5
N-p-tolyl-3a,4,5,7a-tetrahydro-5,7a-epoxy-3,4-propanoisoindoline

Guidance literature:: With In(OSO₂CF₃)3; for 0.333333h; Irradiation; microwave;
DOI:10.1016/S0040-4039(00)01513-6

Reference yield:

: 3139-27-3
N-((furane-2-yl)methyl)-4-methylbenzeneamine

: 108181-33-5
N-p-tolyl-3a,4,5,7a-tetrahydro-5,7a-epoxy-3,4-propanoisoindoline

Guidance literature:: Multi-step reaction with 2 steps

1: 20 percent / In(OTf)3 / 0.13 h / Irradiation; microwave

2: 15 percent / In(OTf)3 / 0.33 h / Irradiation; microwave

With In(OSO₂CF₃)3; 1: intramolecular Diels-Alder reaction / 2: intramolecular Diels-Alder reaction;
DOI:10.1016/S0040-4039(00)01513-6