-2-<(benzyloxycarbonyl)amino>-4-(2-methylphenyl)-3-butenoic acid

Base Information

Chemical Name:-2-<(benzyloxycarbonyl)amino>-4-(2-methylphenyl)-3-butenoic acid
CAS No.:212832-73-0
Molecular Formula:C₁₉H₁₉NO₄
Molecular Weight:325.364
Hs Code.:

<S-(E)>-2-<(benzyloxycarbonyl)amino>-4-(2-methylphenyl)-3-butenoic acid

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Chemical Property of -2-<(benzyloxycarbonyl)amino>-4-(2-methylphenyl)-3-butenoic acid

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Technology Process of -2-<(benzyloxycarbonyl)amino>-4-(2-methylphenyl)-3-butenoic acid

There total 1 articles about -2-<(benzyloxycarbonyl)amino>-4-(2-methylphenyl)-3-butenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 615-37-2
ortho-methylphenyl iodide

: 75266-42-1
(S)-2-<(benzyloxycarbonyl)amino>-3-butenoic acid

: 212832-73-0
-2-<(benzyloxycarbonyl)amino>-4-(2-methylphenyl)-3-butenoic acid

Guidance literature:: With palladium diacetate; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; at 45 ℃; for 24h;
DOI:10.1248/cpb.46.1094

Reference yield: 60.0%

: 212832-73-0
-2-<(benzyloxycarbonyl)amino>-4-(2-methylphenyl)-3-butenoic acid

: 18107-18-1
diazomethyl-trimethyl-silane

: 212832-85-4
-2-<(benzyloxycarbonyl)amino>-4-(2-methylphenyl)-3-butenoic acid methyl ester

Guidance literature:: In methanol; hexane; benzene;
DOI:10.1248/cpb.46.1094

Reference yield:

: 212832-73-0
-2-<(benzyloxycarbonyl)amino>-4-(2-methylphenyl)-3-butenoic acid

: (S)-α-<(methoxycarbonyl)amino>-2-methylbenzenebutanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / hexane; methanol; benzene

2: H₂, 0.1 N aq. HCl / 10 percent Pd/C / methanol

3: aq. NaHCO₃ / dioxane / 5 h / Ambient temperature

With hydrogenchloride; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In 1,4-dioxane; methanol; hexane; benzene;
DOI:10.1248/cpb.46.1094