C₁₆H₂₄N₂O₄

Base Information

• Chemical Name: C₁₆H₂₄N₂O₄
• CAS No.: 1312928-08-7
• Molecular Formula: C₁₆H₂₄N₂O₄
• Molecular Weight: 308.378
• Mol file: 1312928-08-7.mol

Synonyms:

Chemical Property of C₁₆H₂₄N₂O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₆H₂₄N₂O₄

There total 3 articles about C₁₆H₂₄N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C24H30N2O6 (1312927-86-8) → C16H24N2O4 (1312928-08-7)

Guidance literature:

With pyridine; palladium 10% on activated carbon; hydrogen; In methanol;

DOI:10.1021/jm1016126

Reference yield:

C19H21NO5 (1312927-85-7) → C16H24N2O4 (1312928-08-7)

Guidance literature:

Multi-step reaction with 2 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2: pyridine; palladium 10% on activated carbon; hydrogen / methanol

With pyridine; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In methanol; N,N-dimethyl-formamide;

DOI:10.1021/jm1016126

Reference yield:

β-amino-α-methyl propionic acid methyl ester (14678-48-9) → C16H24N2O4 (1312928-08-7)

Guidance literature:

Multi-step reaction with 2 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2: pyridine; palladium 10% on activated carbon; hydrogen / methanol

With pyridine; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In methanol; N,N-dimethyl-formamide;

DOI:10.1021/jm1016126

upstream raw materials:

C₁₉H₂₁NO₅

C₂₄H₃₀N₂O₆

β-amino-α-methyl propionic acid methyl ester

Downstream raw materials:

C₃₁H₅₂N₂O₅

C₃₄H₅₇N₃O₆

C₃₃H₅₅N₃O₆

C₃₂H₅₄N₂O₅