diethyl 6a,9a-dihydroxy-1,6-diphenyl-6,6a,7,8,9,9a-hexahydro-1H-2,5-dioxacyclohepta-as-indacene-1,6-dicarboxylate

Base Information

Chemical Name:diethyl 6a,9a-dihydroxy-1,6-diphenyl-6,6a,7,8,9,9a-hexahydro-1H-2,5-dioxacyclohepta-as-indacene-1,6-dicarboxylate
CAS No.:129579-55-1
Molecular Formula:C₃₁H₃₀O₈
Molecular Weight:530.574
Hs Code.:

diethyl 6a,9a-dihydroxy-1,6-diphenyl-6,6a,7,8,9,9a-hexahydro-1H-2,5-dioxacyclohepta<jkl>-as-indacene-1,6-dicarboxylate

Synonyms:

Suppliers and Price of diethyl 6a,9a-dihydroxy-1,6-diphenyl-6,6a,7,8,9,9a-hexahydro-1H-2,5-dioxacyclohepta-as-indacene-1,6-dicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of diethyl 6a,9a-dihydroxy-1,6-diphenyl-6,6a,7,8,9,9a-hexahydro-1H-2,5-dioxacyclohepta-as-indacene-1,6-dicarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of diethyl 6a,9a-dihydroxy-1,6-diphenyl-6,6a,7,8,9,9a-hexahydro-1H-2,5-dioxacyclohepta-as-indacene-1,6-dicarboxylate

There total 3 articles about diethyl 6a,9a-dihydroxy-1,6-diphenyl-6,6a,7,8,9,9a-hexahydro-1H-2,5-dioxacyclohepta-as-indacene-1,6-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 129579-27-7,129579-48-2
diethyl 2,2'-(5,9-dioxo-6,7,8,9-tetrahydro-5H-benzocycloheptene-1,4-diyloxy)-2,2'-diphenyldiacetate

: 129579-32-4
1,6-diphenyl-8,9-dihydro-7H-2,5-dioxacyclohepta-as-indacene

: 129579-55-1
diethyl 6a,9a-dihydroxy-1,6-diphenyl-6,6a,7,8,9,9a-hexahydro-1H-2,5-dioxacyclohepta-as-indacene-1,6-dicarboxylate

Guidance literature:: With potassium hydroxide; In 1,4-dioxane; for 2.5h; Heating;

Reference yield:

: 13289-90-2
1,4-dihydroxy-6,7,8,9-tetrahydro-5H-benzocycloheptene-5,9-dione

: 129579-55-1
diethyl 6a,9a-dihydroxy-1,6-diphenyl-6,6a,7,8,9,9a-hexahydro-1H-2,5-dioxacyclohepta-as-indacene-1,6-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / K₃PO₄ / dioxane / 3.5 h / 30 °C

2: 33 percent / KOH / dioxane / 2.5 h / Heating

With potassium hydroxide; potassium phosphate; In 1,4-dioxane;

Reference yield:

: 2882-19-1,2216-90-2
ethyl 2-phenyl-2-bromoacetate

: 129579-55-1
diethyl 6a,9a-dihydroxy-1,6-diphenyl-6,6a,7,8,9,9a-hexahydro-1H-2,5-dioxacyclohepta-as-indacene-1,6-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / K₃PO₄ / dioxane / 3.5 h / 30 °C

2: 33 percent / KOH / dioxane / 2.5 h / Heating

With potassium hydroxide; potassium phosphate; In 1,4-dioxane;