4-Methyl-1,4-dihydro-1,3-diphenyl-1,2,4-benzotriazin

Base Information

Chemical Name:4-Methyl-1,4-dihydro-1,3-diphenyl-1,2,4-benzotriazin
CAS No.:74172-94-4
Molecular Formula:C₂₀H₁₇N₃
Molecular Weight:299.375
Hs Code.:

Synonyms:

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Chemical Property of 4-Methyl-1,4-dihydro-1,3-diphenyl-1,2,4-benzotriazin

Chemical Property:

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Technology Process of 4-Methyl-1,4-dihydro-1,3-diphenyl-1,2,4-benzotriazin

There total 4 articles about 4-Methyl-1,4-dihydro-1,3-diphenyl-1,2,4-benzotriazin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13136-18-0
N,N'-diphenylbenzenecarbohydrazonamide

: 74172-94-4
4-Methyl-1,4-dihydro-1,3-diphenyl-1,2,4-benzotriazin

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / HgO / ethanol / 1) reflux, 1 h, 2) room temp., 4 d

2: 1) H₂, 2) BaO, Ba(OH)2 * 8 H₂O / 1) 5percent PdO/BaSO₄ / 1) DMF, 2) room temp., 12 h

With barium dihydroxide; hydrogen; mercury(II) oxide; barium(II) oxide; barium sulfate; trimethyleneglycol; In ethanol;

Reference yield:

: 54367-86-1
C₁₉H₁₅N₃

: 74172-94-4
4-Methyl-1,4-dihydro-1,3-diphenyl-1,2,4-benzotriazin

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylsulfoxide / 140 °C

2: 1) H₂, 2) BaO, Ba(OH)2 * 8 H₂O / 1) 5percent PdO/BaSO₄ / 1) DMF, 2) room temp., 12 h

With barium dihydroxide; hydrogen; barium(II) oxide; barium sulfate; trimethyleneglycol; In dimethyl sulfoxide;

Reference yield:

: 19818-44-1
1,4-Dihydro-1,3-diphenyl-1,2,4-benzotriazin

: 74172-94-4
4-Methyl-1,4-dihydro-1,3-diphenyl-1,2,4-benzotriazin

Guidance literature:: Multi-step reaction with 2 steps

1: HgO / ethanol / 0.5 h

2: 1) H₂, 2) BaO, Ba(OH)2 * 8 H₂O / 1) 5percent PdO/BaSO₄ / 1) DMF, 2) room temp., 12 h

With barium dihydroxide; hydrogen; mercury(II) oxide; barium(II) oxide; barium sulfate; trimethyleneglycol; In ethanol;