C₁₀H₈F₂N₂O₃S

Base Information

Chemical Name:C₁₀H₈F₂N₂O₃S
CAS No.:1392430-07-7
Molecular Formula:C₁₀H₈F₂N₂O₃S
Molecular Weight:274.248
Hs Code.:

C<sub>10</sub>H<sub>8</sub>F<sub>2</sub>N<sub>2</sub>O<sub>3</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₀H₈F₂N₂O₃S

Chemical Property:

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Technology Process of C₁₀H₈F₂N₂O₃S

There total 8 articles about C₁₀H₈F₂N₂O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₁₆F₂N₂O₅S

: 1392430-07-7
C₁₀H₈F₂N₂O₃S

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 2h;
DOI:10.1002/bkcs.10917

Reference yield:

: 260552-98-5
2,6-difluoro-3-nitrobenzoic acid chloride

: 1392430-07-7
C₁₀H₈F₂N₂O₃S

Guidance literature:: Multi-step reaction with 5 steps

1: sodium azide / dichloromethane / 0.5 h / 20 °C

2: dichloromethane / 3 h / Reflux

3: hydrogen; palladium on activated charcoal / methanol / 20 °C

4: pyridine / dichloromethane / 2 h / 20 °C

5: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C

With pyridine; hydrogenchloride; sodium azide; palladium on activated charcoal; hydrogen; In 1,4-dioxane; methanol; dichloromethane; 2: |Curtius Rearrangement;
DOI:10.1002/bkcs.10917

Reference yield:

: 2,6-difluoro-3-nitro-benzoyl azide

: 1392430-07-7
C₁₀H₈F₂N₂O₃S

Guidance literature:: Multi-step reaction with 4 steps

1: dichloromethane / 3 h / Reflux

2: hydrogen; palladium on activated charcoal / methanol / 20 °C

3: pyridine / dichloromethane / 2 h / 20 °C

4: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C

With pyridine; hydrogenchloride; palladium on activated charcoal; hydrogen; In 1,4-dioxane; methanol; dichloromethane; 1: |Curtius Rearrangement;
DOI:10.1002/bkcs.10917