2-Chloro-4-{(2S,3S)-3-[(R)-1-(4-nitro-benzyloxycarbonyloxy)-ethyl]-4-oxo-1-phenylsulfanyl-azetidin-2-yl}-3-phenylsulfanyl-butyric acid 4-nitro-benzyl ester

Base Information

• Chemical Name: 2-Chloro-4-{(2S,3S)-3-[(R)-1-(4-nitro-benzyloxycarbonyloxy)-ethyl]-4-oxo-1-phenylsulfanyl-azetidin-2-yl}-3-phenylsulfanyl-butyric acid 4-nitro-benzyl ester
• CAS No.: 87585-86-2
• Molecular Formula: C₃₆H₃₂ClN₃O₁₀S₂
• Molecular Weight: 766.249

Synonyms:

Chemical Property of 2-Chloro-4-{(2S,3S)-3-[(R)-1-(4-nitro-benzyloxycarbonyloxy)-ethyl]-4-oxo-1-phenylsulfanyl-azetidin-2-yl}-3-phenylsulfanyl-butyric acid 4-nitro-benzyl ester

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Technology Process of 2-Chloro-4-{(2S,3S)-3-[(R)-1-(4-nitro-benzyloxycarbonyloxy)-ethyl]-4-oxo-1-phenylsulfanyl-azetidin-2-yl}-3-phenylsulfanyl-butyric acid 4-nitro-benzyl ester

There total 1 articles about 2-Chloro-4-{(2S,3S)-3-[(R)-1-(4-nitro-benzyloxycarbonyloxy)-ethyl]-4-oxo-1-phenylsulfanyl-azetidin-2-yl}-3-phenylsulfanyl-butyric acid 4-nitro-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+/-)-3(R*)-(1(S*)((((p-nitrobenzyl)oxy)carbonyl)oxy)ethyl)-4(R*)-(3-(((p-nitrobenzyl)oxy)carbonyl)-2-propenyl)azetidin-2-one (87568-62-5) + benzenesulfenyl chloride (931-59-9) → (+/-)-3(R*)-(1(S*)-((((p-nitrobenzyl)oxy)carbonyl)oxy)ethyl)-4(R*)-(3-(((p-nitrobenzyl)oxy)carbonyl)-2-chloro-3-(phenylthio)propyl)azetidin-2-one (87568-65-8) + (+/-)-3(R*)-(1(S*)-((((p-nitrobenzyl)oxy)carbonyl)oxy)ethyl)-4(R*)-(3-(((p-nitrobenzyl)oxy)carbonyl)-3-chloro-2-(phenylthio)propyl)azetidin-2-one (87568-64-7) + 3-Chloro-4-{(2S,3S)-3-[(R)-1-(4-nitro-benzyloxycarbonyloxy)-ethyl]-4-oxo-1-phenylsulfanyl-azetidin-2-yl}-2-phenylsulfanyl-butyric acid 4-nitro-benzyl ester (87568-63-6) + 2-Chloro-4-{(2S,3S)-3-[(R)-1-(4-nitro-benzyloxycarbonyloxy)-ethyl]-4-oxo-1-phenylsulfanyl-azetidin-2-yl}-3-phenylsulfanyl-butyric acid 4-nitro-benzyl ester (87585-86-2)

Guidance literature:

In acetonitrile; for 1h; Title compound not separated from byproducts; Ambient temperature;

DOI:10.1021/ja00363a023

upstream raw materials:

(+/-)-3(R*)-(1(S*)((((p-nitrobenzyl)oxy)carbonyl)oxy)ethyl)-4(R*)-(3-(((p-nitrobenzyl)oxy)carbonyl)-2-propenyl)azetidin-2-one

benzenesulfenyl chloride

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