[(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)Fe(CO)(P(C₆H₅)3)(C₅H₅)]⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)Fe(CO)(P(C₆H₅)3)(C₅H₅)]O₃SCF₃

Base Information

• Chemical Name: [(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)Fe(CO)(P(C₆H₅)3)(C₅H₅)]⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)Fe(CO)(P(C₆H₅)3)(C₅H₅)]O₃SCF₃
• CAS No.: 852834-75-4
• Molecular Formula: CF₃O₃S*C₃₉H₂₉Fe₂N₅O₃P
• Molecular Weight: 907.429

Synonyms:

Chemical Property of [(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)Fe(CO)(P(C₆H₅)3)(C₅H₅)]⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)Fe(CO)(P(C₆H₅)3)(C₅H₅)]O₃SCF₃

Chemical Property:

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Technology Process of [(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)Fe(CO)(P(C₆H₅)3)(C₅H₅)]⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)Fe(CO)(P(C₆H₅)3)(C₅H₅)]O₃SCF₃

There total 1 articles about [(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)Fe(CO)(P(C₆H₅)3)(C₅H₅)]⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)Fe(CO)(P(C₆H₅)3)(C₅H₅)]O₃SCF₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

[(C5H5)(CO)2Fe(N4CC6H4CN)] (463945-92-8) + [(C5H5)(CO)(P(C6H5)3)Fe(C4H8O)](1+)*O3SCF3(1-)=[(C5H5)(CO)(P(C6H5)3)Fe(C4H8O)](O3SCF3) (463945-72-4) → [(C5H5)(CO)2Fe(N4CC6H4CN)Fe(CO)(P(C6H5)3)(C5H5)](1+)*O3SCF3(1-)=[(C5H5)(CO)2Fe(N4CC6H4CN)Fe(CO)(P(C6H5)3)(C5H5)]O3SCF3 (852834-75-4)

Guidance literature:

In dichloromethane; (Ar); Schlenk technique; mixt. of Fe complexes in CH2Cl2 was stirred for18 h; IR monitoring; filtered on Celite; evapd.; chromd. (alumina, CH2Cl2, CH3CN/CH2Cl2, 1/1); elem. anal.;

DOI:10.1016/j.jorganchem.2004.12.007

Reference yield: 87.0%

[(C5H5)(CO)2Fe(N4CC6H4CN)Fe(CO)(P(C6H5)3)(C5H5)](1+)*O3SCF3(1-)=[(C5H5)(CO)2Fe(N4CC6H4CN)Fe(CO)(P(C6H5)3)(C5H5)]O3SCF3 (852834-75-4) + methyl trifluoromethanesulfonate (333-27-7) → [(C5H5)(CO)2Fe((CH3)N4CC6H4CN)Fe(CO)(P(C6H5)3)(C5H5)](2+)*2O3SCF3(1-)=[C40H32Fe2N5O3P](CF3SO3)2

Guidance literature:

In dichloromethane; (Ar); Schlenk technique; soln. of Fe complex in CH2Cl2 was treated with CH3O3SCF3 with stirring at -50°C for 30 min; mixt. was warmed to room temp. and stirred for 4 h; IR monitoring; filtered on Celite; solvent removed (vac.); crystd. (CH2Cl2/Et2O); elem. anal.;

DOI:10.1016/j.jorganchem.2004.12.007

Reference yield: 70.0%

[(C5H5)(CO)2Fe(N4CC6H4CN)Fe(CO)(P(C6H5)3)(C5H5)](1+)*O3SCF3(1-)=[(C5H5)(CO)2Fe(N4CC6H4CN)Fe(CO)(P(C6H5)3)(C5H5)]O3SCF3 (852834-75-4) + trifluorormethanesulfonic acid (1493-13-6) → [(C5H5)(CO)2Fe(HN4CC6H4CN)Fe(CO)(P(C6H5)3)(C5H5)](2+)*2O3SCF3(1-)=[(C5H5)(CO)2Fe(C8H5N5)Fe(CO)(P(C6H5)3)(C5H5)](O3SCF3)2

Guidance literature:

In dichloromethane; (Ar); Schlenk technique; acid was added to stirred soln. of Fe complex in CH2Cl2 at -60°C; after 30 min mixt. was warmed to room temp. and stirred for 4 h; IR monitoring; solvent removed (vac.); redissolved in CH2Cl2; layered with Et2O; elem. anal.;

DOI:10.1016/j.jorganchem.2004.12.007

upstream raw materials:

[(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)]

[(C₅H₅)(CO)(P(C₆H₅)3)Fe(C₄H₈O)]⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₅H₅)(CO)(P(C₆H₅)3)Fe(C₄H₈O)](O₃SCF₃)

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