2',3'-O-dibenzoyl-3-<11-<(4-monomethoxytrityl)thio>undecyl>uridine 5'-<(2-cyanoethyl) diisopropylamino phosphite>

Base Information

Chemical Name:2',3'-O-dibenzoyl-3-<11-<(4-monomethoxytrityl)thio>undecyl>uridine 5'-<(2-cyanoethyl) diisopropylamino phosphite>
CAS No.:130518-74-0
Molecular Formula:C₆₃H₇₅N₄O₁₀PS
Molecular Weight:1111.35
Hs Code.:

Synonyms:

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Chemical Property of 2',3'-O-dibenzoyl-3-<11-<(4-monomethoxytrityl)thio>undecyl>uridine 5'-<(2-cyanoethyl) diisopropylamino phosphite>

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Technology Process of 2',3'-O-dibenzoyl-3-<11-<(4-monomethoxytrityl)thio>undecyl>uridine 5'-<(2-cyanoethyl) diisopropylamino phosphite>

There total 3 articles about 2',3'-O-dibenzoyl-3-<11-<(4-monomethoxytrityl)thio>undecyl>uridine 5'-<(2-cyanoethyl) diisopropylamino phosphite> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 130518-71-7
11-<(4-methoxytrityl)thio>undecanol

: 130518-74-0,130530-61-9
2',3'-O-dibenzoyl-3-<11-<(4-monomethoxytrityl)thio>undecyl>uridine 5'-<(2-cyanoethyl) diisopropylamino phosphite>

Guidance literature:: Multi-step reaction with 3 steps

1: 950 mg / pyridine / 3 h / Ambient temperature

2: 1) K₂CO₃, 2) dichloroacetic acid / 1) DMSO, r.t., 24 h, 2) CH₂Cl₂, r.t., 5 min

3: 860 mg / diisopropylammonium tetrazolide / CH₂Cl₂ / 3 h / Ambient temperature

With pyridine; dichloro-acetic acid; N,N-diisopropylamine tetrazolide; potassium carbonate; In dichloromethane;
DOI:10.1002/hlca.19900730434

Reference yield:

: 130518-72-8
11-<(4-monomethoxytrityl)thio>undecyl 4-toluenesulfonate

: 130518-74-0,130530-61-9
2',3'-O-dibenzoyl-3-<11-<(4-monomethoxytrityl)thio>undecyl>uridine 5'-<(2-cyanoethyl) diisopropylamino phosphite>

Guidance literature:: Multi-step reaction with 2 steps

1: 1) K₂CO₃, 2) dichloroacetic acid / 1) DMSO, r.t., 24 h, 2) CH₂Cl₂, r.t., 5 min

2: 860 mg / diisopropylammonium tetrazolide / CH₂Cl₂ / 3 h / Ambient temperature

With dichloro-acetic acid; N,N-diisopropylamine tetrazolide; potassium carbonate; In dichloromethane;
DOI:10.1002/hlca.19900730434