sodium 3,5-di-tert-butyl-o-benzosemiquinolate

Base Information

Chemical Name:sodium 3,5-di-tert-butyl-o-benzosemiquinolate
CAS No.:4679-12-3
Molecular Formula:C₁₄H₂₀O₂*Na
Molecular Weight:243.301
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of sodium 3,5-di-tert-butyl-o-benzosemiquinolate

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Technology Process of sodium 3,5-di-tert-butyl-o-benzosemiquinolate

There total 1 articles about sodium 3,5-di-tert-butyl-o-benzosemiquinolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3383-21-9
3,5-di-tert-butyl-o-benzoquinone

: 4679-12-3,61373-02-2
sodium 3,5-di-tert-butyl-o-benzosemiquinolate

Guidance literature:: Multistep reaction; (i) /BRN= 2047944/, Na, Et₂O, (ii) /BRN= 2047944/;

Reference yield: 87.0%

: 13314-53-9
diethylgermanium dibromide

: 4679-12-3,61373-02-2
disodium 3,5-di-t-butyl-1,2-pyrocatecholate

: 78100-52-4
2,2-diethyl(6,8-di-tert-butyl)-4,5-benzo-2-germa-1,3-dioxolane

: 7647-15-6
sodium bromide

Guidance literature:: In diethyl ether; 3 h at 20°C; NaBr washed out (water); ether evapd.; recrystd. (acetonitrile); elem. anal.;
DOI:10.1007/BF00962274

Reference yield: 84.0%

: Pd₂(azobenzene)₂Cl₂

: 4679-12-3,61373-02-2
sodium 3,5-di-tert-butyl-o-benzosemiquinolate

: 2-(phenylazo)phenylpalladium 3,5-di-tert-butyl-1,2-benzosemiquinolate

Guidance literature:: In tetrahydrofuran; byproducts: NaCl; soln. of sodium 3,5-di-tert-butyl-1,2-benzosemiquinolate added to suspn. of ((C6H5NNC6H4)PdCl)2 in THF; THF removed in vac.; ppt. repeatedly washed with hexane; evapd.; elem. anal.;
DOI:10.1007/BF00949213