Technology Process of C24H27(2)H10N
There total 12 articles about C24H27(2)H10N which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 74 percent / PPS / 6 h / 80 °C
2: 31 percent / SeO2 / dioxane; H2O / 12 h / Heating
3: 58 percent / benzene / 1) 1 h, reflux; 2 h, room temp.
4: 33 percent / CH3OD/NaOD/NaBH4 / 6 h / Heating
5: diethyl ether / 0.25 h / 0 °C
6: 1) LiAlH4, 2) MnO2 / 1) Ether, 15 min, -78 deg C; 1 h, -40 deg C, 2) hexane, 2.5 h, 0 deg C
7: CDCl3 / 2.5 h
With
manganese(IV) oxide; sodium tetrahydroborate; lithium aluminium tetrahydride; selenium(IV) oxide; deuteriated sodium hydroxide; deuteromethanol; PPS;
In
1,4-dioxane; diethyl ether; chloroform-d1; water; benzene;
DOI:10.1002/jlac.198519851013
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 74 percent / PPS / 6 h / 80 °C
2: 31 percent / SeO2 / dioxane; H2O / 12 h / Heating
3: 58 percent / benzene / 1) 1 h, reflux; 2 h, room temp.
4: 33 percent / CH3OD/NaOD/NaBH4 / 6 h / Heating
5: diethyl ether / 0.25 h / 0 °C
6: 1) LiAlH4, 2) MnO2 / 1) Ether, 15 min, -78 deg C; 1 h, -40 deg C, 2) hexane, 2.5 h, 0 deg C
7: CDCl3 / 1 h
With
manganese(IV) oxide; sodium tetrahydroborate; lithium aluminium tetrahydride; selenium(IV) oxide; deuteriated sodium hydroxide; deuteromethanol; PPS;
In
1,4-dioxane; diethyl ether; chloroform-d1; water; benzene;
DOI:10.1002/jlac.198519851013
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 31 percent / SeO2 / dioxane; H2O / 12 h / Heating
2: 58 percent / benzene / 1) 1 h, reflux; 2 h, room temp.
3: 33 percent / CH3OD/NaOD/NaBH4 / 6 h / Heating
4: diethyl ether / 0.25 h / 0 °C
5: 1) LiAlH4, 2) MnO2 / 1) Ether, 15 min, -78 deg C; 1 h, -40 deg C, 2) hexane, 2.5 h, 0 deg C
6: CDCl3 / 2.5 h
With
manganese(IV) oxide; sodium tetrahydroborate; lithium aluminium tetrahydride; selenium(IV) oxide; deuteriated sodium hydroxide; deuteromethanol;
In
1,4-dioxane; diethyl ether; chloroform-d1; water; benzene;
DOI:10.1002/jlac.198519851013